Pechini method used in the obtention of semiconductor nanoparticles based niobium

The (Nb2O5) niobium pentoxide compound was synthetized by Pechini method. The followed synthesis protocol is promising to obtain 2O5 nanoparticles, in orthorhombic phase. This phase was obtained in the samples calcined at 600°C for 2 hours and the submitted at 500°C for 22 hours in gas flow. For the...