Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes

This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naran...

Full description

Autores:
Caballero Galván, Ashley Sthefanía
Tipo de recurso:
Fecha de publicación:
2017
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/63889
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/63889
http://bdigital.unal.edu.co/64508/
Palabra clave:
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Extracción asistida por ultrasonido
Extracción con fluidos supercríticos
Residuos agroindustriales
Biorefinerías
Compuestos polifenólicos
Ultrasound assisted extraction
Supercritical fluid extraction
Agroindustrial waste
Biorefineries
Polyphenolic compounds
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
id UNACIONAL2_4559a2a39d4ccf71ef8d01893bfbf42f
oai_identifier_str oai:repositorio.unal.edu.co:unal/63889
network_acronym_str UNACIONAL2
network_name_str Universidad Nacional de Colombia
repository_id_str
dc.title.spa.fl_str_mv Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
title Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
spellingShingle Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Extracción asistida por ultrasonido
Extracción con fluidos supercríticos
Residuos agroindustriales
Biorefinerías
Compuestos polifenólicos
Ultrasound assisted extraction
Supercritical fluid extraction
Agroindustrial waste
Biorefineries
Polyphenolic compounds
title_short Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
title_full Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
title_fullStr Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
title_full_unstemmed Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
title_sort Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
dc.creator.fl_str_mv Caballero Galván, Ashley Sthefanía
dc.contributor.advisor.spa.fl_str_mv Cardona Alzate, Carlos Ariel
dc.contributor.author.spa.fl_str_mv Caballero Galván, Ashley Sthefanía
dc.subject.ddc.spa.fl_str_mv 66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
topic 66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Extracción asistida por ultrasonido
Extracción con fluidos supercríticos
Residuos agroindustriales
Biorefinerías
Compuestos polifenólicos
Ultrasound assisted extraction
Supercritical fluid extraction
Agroindustrial waste
Biorefineries
Polyphenolic compounds
dc.subject.proposal.spa.fl_str_mv Extracción asistida por ultrasonido
Extracción con fluidos supercríticos
Residuos agroindustriales
Biorefinerías
Compuestos polifenólicos
Ultrasound assisted extraction
Supercritical fluid extraction
Agroindustrial waste
Biorefineries
Polyphenolic compounds
description This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naranjilla peel. Where these residues are produced in larg amount in Colombia. In addition, other raw materials from fruit and olive residues were analyzed. For this experimental stage, the physical-chemical characterization of the raw materials was initially carried out. Subsequently, the extraction conditions of chlorogenic acid was theoretically evaluated, in order to determine the best operating conditions. Then, extractions of the compounds of interest were carried out with technologies such as solvent extraction, Soxhlet extraction, ultrasonic assisted extraction and supercritical fluids extraction. This last was realized using CO2 as supercritical fluid. From this, it was determined the influence of each of these technologies in the polyphenolic compounds extraction. As a results were obtained compounds such as chlorogenic acid, ferulic acid, quercetin, vanillin, among others. In addition, these raw materials were used in integrated processes, through the development of different biorefineries. In these analysis were obtained of value-added products such as antioxidants, ethanol, xylitol, furfural and energy generation. Where, the economical, energetic and environmental aspects were evaluated (Texto tomado de la fuente)
publishDate 2017
dc.date.issued.spa.fl_str_mv 2017
dc.date.accessioned.spa.fl_str_mv 2019-07-02T22:15:39Z
dc.date.available.spa.fl_str_mv 2019-07-02T22:15:39Z
dc.type.spa.fl_str_mv Trabajo de grado - Maestría
dc.type.driver.spa.fl_str_mv info:eu-repo/semantics/masterThesis
dc.type.version.spa.fl_str_mv info:eu-repo/semantics/acceptedVersion
dc.type.content.spa.fl_str_mv Text
dc.type.redcol.spa.fl_str_mv http://purl.org/redcol/resource_type/TM
status_str acceptedVersion
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/63889
dc.identifier.eprints.spa.fl_str_mv http://bdigital.unal.edu.co/64508/
url https://repositorio.unal.edu.co/handle/unal/63889
http://bdigital.unal.edu.co/64508/
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Sede Manizales Facultad de Ingeniería y Arquitectura Departamento de Ingeniería Química
Departamento de Ingeniería Química
dc.relation.references.spa.fl_str_mv Caballero Galván, Ashley Sthefanía (2017) Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes. Maestría thesis, Universidad Nacional de Colombia - Sede Manizales.
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.spa.fl_str_mv application/pdf
institution Universidad Nacional de Colombia
bitstream.url.fl_str_mv https://repositorio.unal.edu.co/bitstream/unal/63889/1/1090176288.2017.pdf
https://repositorio.unal.edu.co/bitstream/unal/63889/2/1090176288.2017.pdf.jpg
bitstream.checksum.fl_str_mv 6a63980f9151cc17deb33dce81e6b7d6
3641be87a350765292bf468b8e460997
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositorio Institucional Universidad Nacional de Colombia
repository.mail.fl_str_mv repositorio_nal@unal.edu.co
_version_ 1814089690555351040
spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Cardona Alzate, Carlos Arielbd4aaf0b-7e59-4ce2-8cb4-66475cd35001Caballero Galván, Ashley Sthefaníae5912049-5b8d-4a26-900d-616abb8f83dd3002019-07-02T22:15:39Z2019-07-02T22:15:39Z2017https://repositorio.unal.edu.co/handle/unal/63889http://bdigital.unal.edu.co/64508/This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naranjilla peel. Where these residues are produced in larg amount in Colombia. In addition, other raw materials from fruit and olive residues were analyzed. For this experimental stage, the physical-chemical characterization of the raw materials was initially carried out. Subsequently, the extraction conditions of chlorogenic acid was theoretically evaluated, in order to determine the best operating conditions. Then, extractions of the compounds of interest were carried out with technologies such as solvent extraction, Soxhlet extraction, ultrasonic assisted extraction and supercritical fluids extraction. This last was realized using CO2 as supercritical fluid. From this, it was determined the influence of each of these technologies in the polyphenolic compounds extraction. As a results were obtained compounds such as chlorogenic acid, ferulic acid, quercetin, vanillin, among others. In addition, these raw materials were used in integrated processes, through the development of different biorefineries. In these analysis were obtained of value-added products such as antioxidants, ethanol, xylitol, furfural and energy generation. Where, the economical, energetic and environmental aspects were evaluated (Texto tomado de la fuente)Este trabajo demuestra el potencial para obtener compuestos polifenólicos mediante el uso de tecnologías no convencionales: extracción asistida por ultrasonido y extracción de fluidos supercríticos. Las materias primas empleadas para desarrollar el presente trabajo fueron borra de café, zoca de café y cáscara de lulo. Donde estos residuos se producen en gran cantidad en Colombia. Además, se analizaron otras materias primas de residuos de frutas y olivo. Para la etapa experimental, inicialmente se llevó a cabo la caracterización físicoquímica de las materias primas. Posteriormente, fueron evaluadas teóricamente las condiciones de extracción del ácido clorogénico, para determinar las mejores condiciones de operación. Luego, las extracciones de los compuestos de interés fueron llevadas a cabo con tecnologías de extracción por solvente, extracción Soxhlet, extracción asistida por ultrasonidos y extracción de fluidos supercríticos. Esto último fue realizado utilizando CO2 como fluido supercrítico. A partir de esto, fue determinada la influencia de cada una de estas tecnologías en la extracción de compuestos polifenólicos. Como resultado, se obtuvieron compuestos tales como ácido clorogénico, ácido ferúlico, quercetina, vainillina, entre otros. Además, estas materias primas se utilizaron en procesos integrados, a través del desarrollo de diferentes biorrefinerías. En estos análisis se obtuvieron productos de valor agregado como antioxidantes, etanol, xilitol, furfural y generación de energía. Donde se evaluaron los aspectos económicos, energéticos y ambientalesMaestríaapplication/pdfspaUniversidad Nacional de Colombia Sede Manizales Facultad de Ingeniería y Arquitectura Departamento de Ingeniería QuímicaDepartamento de Ingeniería QuímicaCaballero Galván, Ashley Sthefanía (2017) Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes. Maestría thesis, Universidad Nacional de Colombia - Sede Manizales.66 Ingeniería química y Tecnologías relacionadas/ Chemical engineeringExtracción asistida por ultrasonidoExtracción con fluidos supercríticosResiduos agroindustrialesBiorefineríasCompuestos polifenólicosUltrasound assisted extractionSupercritical fluid extractionAgroindustrial wasteBiorefineriesPolyphenolic compoundsEvaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastesTrabajo de grado - Maestríainfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/acceptedVersionTexthttp://purl.org/redcol/resource_type/TMORIGINAL1090176288.2017.pdfTesis de Maestría en Ingeniería - Ingeniería Químicaapplication/pdf5454790https://repositorio.unal.edu.co/bitstream/unal/63889/1/1090176288.2017.pdf6a63980f9151cc17deb33dce81e6b7d6MD51THUMBNAIL1090176288.2017.pdf.jpg1090176288.2017.pdf.jpgGenerated Thumbnailimage/jpeg5689https://repositorio.unal.edu.co/bitstream/unal/63889/2/1090176288.2017.pdf.jpg3641be87a350765292bf468b8e460997MD52unal/63889oai:repositorio.unal.edu.co:unal/638892024-05-01 23:11:41.319Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co