Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes
This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naran...
- Autores:
-
Caballero Galván, Ashley Sthefanía
- Tipo de recurso:
- Fecha de publicación:
- 2017
- Institución:
- Universidad Nacional de Colombia
- Repositorio:
- Universidad Nacional de Colombia
- Idioma:
- spa
- OAI Identifier:
- oai:repositorio.unal.edu.co:unal/63889
- Acceso en línea:
- https://repositorio.unal.edu.co/handle/unal/63889
http://bdigital.unal.edu.co/64508/
- Palabra clave:
- 66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Extracción asistida por ultrasonido
Extracción con fluidos supercríticos
Residuos agroindustriales
Biorefinerías
Compuestos polifenólicos
Ultrasound assisted extraction
Supercritical fluid extraction
Agroindustrial waste
Biorefineries
Polyphenolic compounds
- Rights
- openAccess
- License
- Atribución-NoComercial 4.0 Internacional
id |
UNACIONAL2_4559a2a39d4ccf71ef8d01893bfbf42f |
---|---|
oai_identifier_str |
oai:repositorio.unal.edu.co:unal/63889 |
network_acronym_str |
UNACIONAL2 |
network_name_str |
Universidad Nacional de Colombia |
repository_id_str |
|
dc.title.spa.fl_str_mv |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
title |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
spellingShingle |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes 66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering Extracción asistida por ultrasonido Extracción con fluidos supercríticos Residuos agroindustriales Biorefinerías Compuestos polifenólicos Ultrasound assisted extraction Supercritical fluid extraction Agroindustrial waste Biorefineries Polyphenolic compounds |
title_short |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
title_full |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
title_fullStr |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
title_full_unstemmed |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
title_sort |
Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes |
dc.creator.fl_str_mv |
Caballero Galván, Ashley Sthefanía |
dc.contributor.advisor.spa.fl_str_mv |
Cardona Alzate, Carlos Ariel |
dc.contributor.author.spa.fl_str_mv |
Caballero Galván, Ashley Sthefanía |
dc.subject.ddc.spa.fl_str_mv |
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering |
topic |
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering Extracción asistida por ultrasonido Extracción con fluidos supercríticos Residuos agroindustriales Biorefinerías Compuestos polifenólicos Ultrasound assisted extraction Supercritical fluid extraction Agroindustrial waste Biorefineries Polyphenolic compounds |
dc.subject.proposal.spa.fl_str_mv |
Extracción asistida por ultrasonido Extracción con fluidos supercríticos Residuos agroindustriales Biorefinerías Compuestos polifenólicos Ultrasound assisted extraction Supercritical fluid extraction Agroindustrial waste Biorefineries Polyphenolic compounds |
description |
This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naranjilla peel. Where these residues are produced in larg amount in Colombia. In addition, other raw materials from fruit and olive residues were analyzed. For this experimental stage, the physical-chemical characterization of the raw materials was initially carried out. Subsequently, the extraction conditions of chlorogenic acid was theoretically evaluated, in order to determine the best operating conditions. Then, extractions of the compounds of interest were carried out with technologies such as solvent extraction, Soxhlet extraction, ultrasonic assisted extraction and supercritical fluids extraction. This last was realized using CO2 as supercritical fluid. From this, it was determined the influence of each of these technologies in the polyphenolic compounds extraction. As a results were obtained compounds such as chlorogenic acid, ferulic acid, quercetin, vanillin, among others. In addition, these raw materials were used in integrated processes, through the development of different biorefineries. In these analysis were obtained of value-added products such as antioxidants, ethanol, xylitol, furfural and energy generation. Where, the economical, energetic and environmental aspects were evaluated (Texto tomado de la fuente) |
publishDate |
2017 |
dc.date.issued.spa.fl_str_mv |
2017 |
dc.date.accessioned.spa.fl_str_mv |
2019-07-02T22:15:39Z |
dc.date.available.spa.fl_str_mv |
2019-07-02T22:15:39Z |
dc.type.spa.fl_str_mv |
Trabajo de grado - Maestría |
dc.type.driver.spa.fl_str_mv |
info:eu-repo/semantics/masterThesis |
dc.type.version.spa.fl_str_mv |
info:eu-repo/semantics/acceptedVersion |
dc.type.content.spa.fl_str_mv |
Text |
dc.type.redcol.spa.fl_str_mv |
http://purl.org/redcol/resource_type/TM |
status_str |
acceptedVersion |
dc.identifier.uri.none.fl_str_mv |
https://repositorio.unal.edu.co/handle/unal/63889 |
dc.identifier.eprints.spa.fl_str_mv |
http://bdigital.unal.edu.co/64508/ |
url |
https://repositorio.unal.edu.co/handle/unal/63889 http://bdigital.unal.edu.co/64508/ |
dc.language.iso.spa.fl_str_mv |
spa |
language |
spa |
dc.relation.ispartof.spa.fl_str_mv |
Universidad Nacional de Colombia Sede Manizales Facultad de Ingeniería y Arquitectura Departamento de Ingeniería Química Departamento de Ingeniería Química |
dc.relation.references.spa.fl_str_mv |
Caballero Galván, Ashley Sthefanía (2017) Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes. Maestría thesis, Universidad Nacional de Colombia - Sede Manizales. |
dc.rights.spa.fl_str_mv |
Derechos reservados - Universidad Nacional de Colombia |
dc.rights.coar.fl_str_mv |
http://purl.org/coar/access_right/c_abf2 |
dc.rights.license.spa.fl_str_mv |
Atribución-NoComercial 4.0 Internacional |
dc.rights.uri.spa.fl_str_mv |
http://creativecommons.org/licenses/by-nc/4.0/ |
dc.rights.accessrights.spa.fl_str_mv |
info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Atribución-NoComercial 4.0 Internacional Derechos reservados - Universidad Nacional de Colombia http://creativecommons.org/licenses/by-nc/4.0/ http://purl.org/coar/access_right/c_abf2 |
eu_rights_str_mv |
openAccess |
dc.format.mimetype.spa.fl_str_mv |
application/pdf |
institution |
Universidad Nacional de Colombia |
bitstream.url.fl_str_mv |
https://repositorio.unal.edu.co/bitstream/unal/63889/1/1090176288.2017.pdf https://repositorio.unal.edu.co/bitstream/unal/63889/2/1090176288.2017.pdf.jpg |
bitstream.checksum.fl_str_mv |
6a63980f9151cc17deb33dce81e6b7d6 3641be87a350765292bf468b8e460997 |
bitstream.checksumAlgorithm.fl_str_mv |
MD5 MD5 |
repository.name.fl_str_mv |
Repositorio Institucional Universidad Nacional de Colombia |
repository.mail.fl_str_mv |
repositorio_nal@unal.edu.co |
_version_ |
1814089690555351040 |
spelling |
Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Cardona Alzate, Carlos Arielbd4aaf0b-7e59-4ce2-8cb4-66475cd35001Caballero Galván, Ashley Sthefaníae5912049-5b8d-4a26-900d-616abb8f83dd3002019-07-02T22:15:39Z2019-07-02T22:15:39Z2017https://repositorio.unal.edu.co/handle/unal/63889http://bdigital.unal.edu.co/64508/This work demonstrates the potential for obtaining polyphenolic compounds through the use of unconventional technologies: ultrasound assisted extraction and supercritical fluids extraction. The raw material employed in to develop the present work were spent coffee grounds, coffee cut-stems and naranjilla peel. Where these residues are produced in larg amount in Colombia. In addition, other raw materials from fruit and olive residues were analyzed. For this experimental stage, the physical-chemical characterization of the raw materials was initially carried out. Subsequently, the extraction conditions of chlorogenic acid was theoretically evaluated, in order to determine the best operating conditions. Then, extractions of the compounds of interest were carried out with technologies such as solvent extraction, Soxhlet extraction, ultrasonic assisted extraction and supercritical fluids extraction. This last was realized using CO2 as supercritical fluid. From this, it was determined the influence of each of these technologies in the polyphenolic compounds extraction. As a results were obtained compounds such as chlorogenic acid, ferulic acid, quercetin, vanillin, among others. In addition, these raw materials were used in integrated processes, through the development of different biorefineries. In these analysis were obtained of value-added products such as antioxidants, ethanol, xylitol, furfural and energy generation. Where, the economical, energetic and environmental aspects were evaluated (Texto tomado de la fuente)Este trabajo demuestra el potencial para obtener compuestos polifenólicos mediante el uso de tecnologías no convencionales: extracción asistida por ultrasonido y extracción de fluidos supercríticos. Las materias primas empleadas para desarrollar el presente trabajo fueron borra de café, zoca de café y cáscara de lulo. Donde estos residuos se producen en gran cantidad en Colombia. Además, se analizaron otras materias primas de residuos de frutas y olivo. Para la etapa experimental, inicialmente se llevó a cabo la caracterización físicoquímica de las materias primas. Posteriormente, fueron evaluadas teóricamente las condiciones de extracción del ácido clorogénico, para determinar las mejores condiciones de operación. Luego, las extracciones de los compuestos de interés fueron llevadas a cabo con tecnologías de extracción por solvente, extracción Soxhlet, extracción asistida por ultrasonidos y extracción de fluidos supercríticos. Esto último fue realizado utilizando CO2 como fluido supercrítico. A partir de esto, fue determinada la influencia de cada una de estas tecnologías en la extracción de compuestos polifenólicos. Como resultado, se obtuvieron compuestos tales como ácido clorogénico, ácido ferúlico, quercetina, vainillina, entre otros. Además, estas materias primas se utilizaron en procesos integrados, a través del desarrollo de diferentes biorrefinerías. En estos análisis se obtuvieron productos de valor agregado como antioxidantes, etanol, xilitol, furfural y generación de energía. Donde se evaluaron los aspectos económicos, energéticos y ambientalesMaestríaapplication/pdfspaUniversidad Nacional de Colombia Sede Manizales Facultad de Ingeniería y Arquitectura Departamento de Ingeniería QuímicaDepartamento de Ingeniería QuímicaCaballero Galván, Ashley Sthefanía (2017) Evaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastes. Maestría thesis, Universidad Nacional de Colombia - Sede Manizales.66 Ingeniería química y Tecnologías relacionadas/ Chemical engineeringExtracción asistida por ultrasonidoExtracción con fluidos supercríticosResiduos agroindustrialesBiorefineríasCompuestos polifenólicosUltrasound assisted extractionSupercritical fluid extractionAgroindustrial wasteBiorefineriesPolyphenolic compoundsEvaluation of the influence of ultrasound and supercritical fluids in processes of polyphenolic compounds extraction from agroindustrial wastesTrabajo de grado - Maestríainfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/acceptedVersionTexthttp://purl.org/redcol/resource_type/TMORIGINAL1090176288.2017.pdfTesis de Maestría en Ingeniería - Ingeniería Químicaapplication/pdf5454790https://repositorio.unal.edu.co/bitstream/unal/63889/1/1090176288.2017.pdf6a63980f9151cc17deb33dce81e6b7d6MD51THUMBNAIL1090176288.2017.pdf.jpg1090176288.2017.pdf.jpgGenerated Thumbnailimage/jpeg5689https://repositorio.unal.edu.co/bitstream/unal/63889/2/1090176288.2017.pdf.jpg3641be87a350765292bf468b8e460997MD52unal/63889oai:repositorio.unal.edu.co:unal/638892024-05-01 23:11:41.319Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co |