Caracterization of thin films by x’pert-pro panalytical difractometer

In this work, the structural characterization of thin films using a conventional diffraction equipment, brand X'Pert PRO PANalytical X-rays is described. A brief review of the theoretical diffraction techniques and X-ray reflectivity is included. In the experimental part the conditions necessar...

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Autores:
Tolosa, Jhonny
Ortiz, César A.
Tipo de recurso:
Article of journal
Fecha de publicación:
2014
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/50920
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/50920
http://bdigital.unal.edu.co/44962/
Palabra clave:
Película delgada
Difracción de rayos-X de haz rasante
reflectividad de rayos-X.
Thin films
grazing incidence X-ray diffraction
X-ray reflectivity
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
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oai_identifier_str oai:repositorio.unal.edu.co:unal/50920
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network_name_str Universidad Nacional de Colombia
repository_id_str
spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Tolosa, Jhonnyc5ee67c0-3aff-4c4f-8209-763532f3a14c300Ortiz, César A.8f639299-087c-4008-b856-f71a9784ef043002019-06-29T11:03:47Z2019-06-29T11:03:47Z2014-09-13https://repositorio.unal.edu.co/handle/unal/50920http://bdigital.unal.edu.co/44962/In this work, the structural characterization of thin films using a conventional diffraction equipment, brand X'Pert PRO PANalytical X-rays is described. A brief review of the theoretical diffraction techniques and X-ray reflectivity is included. In the experimental part the conditions necessary for the assembly of the samples were determined on the computer using the settings grazing incidence and X-ray reflectivity. 11 different thin film samples were tested and the results of thickness and lattice parameter were obtained by the X'Pert HighScore Plus and X'pert Reflectivity programs respectively. The results suggest the feasibility of using a conventional X-ray equipment for the characterization of thin films.En este trabajo, se describe la caracterización estructural de películas delgadas empleando un equipo convencional de difracción de rayos-X, X’PERT PRO PANalytical. Se incluye una breve revisión teórica de las técnicas de difracción y reflectividad de rayos –X. En la parte experimental  se determinaron las condiciones necesarias para el montaje de las muestras en el equipo, empleando las configuraciones de incidencia rasante y de reflectividad de rayos-X. Se analizaron 11 muestras diferentes de película delgada y los resultados de espesor y de parámetro de red se obtuvieron mediante los programas X’pert Reflectivity y X´pert HighScore Plus respectivamente. Los resultados obtenidos sugieren la viabilidad de emplear un equipo convencional de rayos-X para la caracterización de películas delgadas.application/pdfspaUniversidad Nacional de Colombia, Bogotáhttp://revistas.unal.edu.co/index.php/momento/article/view/45541Universidad Nacional de Colombia Revistas electrónicas UN MOMENTO - Revista de FísicaMOMENTO - Revista de FísicaMOMENTO - Revista de Física; núm. 48E (2014); 38-51 0121-4470Tolosa, Jhonny and Ortiz, César A. (2014) Caracterization of thin films by x’pert-pro panalytical difractometer. MOMENTO - Revista de Física; núm. 48E (2014); 38-51 0121-4470 .Caracterization of thin films by x’pert-pro panalytical difractometerArtículo de revistainfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1http://purl.org/coar/version/c_970fb48d4fbd8a85Texthttp://purl.org/redcol/resource_type/ARTPelícula delgadaDifracción de rayos-X de haz rasantereflectividad de rayos-X.Thin filmsgrazing incidence X-ray diffractionX-ray reflectivityORIGINAL45541-219564-2-PB.pdfapplication/pdf735969https://repositorio.unal.edu.co/bitstream/unal/50920/1/45541-219564-2-PB.pdf118fd61bb1364265e871363017002aeeMD51THUMBNAIL45541-219564-2-PB.pdf.jpg45541-219564-2-PB.pdf.jpgGenerated Thumbnailimage/jpeg6979https://repositorio.unal.edu.co/bitstream/unal/50920/2/45541-219564-2-PB.pdf.jpg9e5d8e8132b2c9e914c5820f4d47668bMD52unal/50920oai:repositorio.unal.edu.co:unal/509202023-12-17 23:06:01.263Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co
dc.title.spa.fl_str_mv Caracterization of thin films by x’pert-pro panalytical difractometer
title Caracterization of thin films by x’pert-pro panalytical difractometer
spellingShingle Caracterization of thin films by x’pert-pro panalytical difractometer
Película delgada
Difracción de rayos-X de haz rasante
reflectividad de rayos-X.
Thin films
grazing incidence X-ray diffraction
X-ray reflectivity
title_short Caracterization of thin films by x’pert-pro panalytical difractometer
title_full Caracterization of thin films by x’pert-pro panalytical difractometer
title_fullStr Caracterization of thin films by x’pert-pro panalytical difractometer
title_full_unstemmed Caracterization of thin films by x’pert-pro panalytical difractometer
title_sort Caracterization of thin films by x’pert-pro panalytical difractometer
dc.creator.fl_str_mv Tolosa, Jhonny
Ortiz, César A.
dc.contributor.author.spa.fl_str_mv Tolosa, Jhonny
Ortiz, César A.
dc.subject.proposal.spa.fl_str_mv Película delgada
Difracción de rayos-X de haz rasante
reflectividad de rayos-X.
Thin films
grazing incidence X-ray diffraction
X-ray reflectivity
topic Película delgada
Difracción de rayos-X de haz rasante
reflectividad de rayos-X.
Thin films
grazing incidence X-ray diffraction
X-ray reflectivity
description In this work, the structural characterization of thin films using a conventional diffraction equipment, brand X'Pert PRO PANalytical X-rays is described. A brief review of the theoretical diffraction techniques and X-ray reflectivity is included. In the experimental part the conditions necessary for the assembly of the samples were determined on the computer using the settings grazing incidence and X-ray reflectivity. 11 different thin film samples were tested and the results of thickness and lattice parameter were obtained by the X'Pert HighScore Plus and X'pert Reflectivity programs respectively. The results suggest the feasibility of using a conventional X-ray equipment for the characterization of thin films.
publishDate 2014
dc.date.issued.spa.fl_str_mv 2014-09-13
dc.date.accessioned.spa.fl_str_mv 2019-06-29T11:03:47Z
dc.date.available.spa.fl_str_mv 2019-06-29T11:03:47Z
dc.type.spa.fl_str_mv Artículo de revista
dc.type.coar.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
dc.type.driver.spa.fl_str_mv info:eu-repo/semantics/article
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dc.type.content.spa.fl_str_mv Text
dc.type.redcol.spa.fl_str_mv http://purl.org/redcol/resource_type/ART
format http://purl.org/coar/resource_type/c_6501
status_str publishedVersion
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/50920
dc.identifier.eprints.spa.fl_str_mv http://bdigital.unal.edu.co/44962/
url https://repositorio.unal.edu.co/handle/unal/50920
http://bdigital.unal.edu.co/44962/
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.spa.fl_str_mv http://revistas.unal.edu.co/index.php/momento/article/view/45541
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Revistas electrónicas UN MOMENTO - Revista de Física
MOMENTO - Revista de Física
dc.relation.ispartofseries.none.fl_str_mv MOMENTO - Revista de Física; núm. 48E (2014); 38-51 0121-4470
dc.relation.references.spa.fl_str_mv Tolosa, Jhonny and Ortiz, César A. (2014) Caracterization of thin films by x’pert-pro panalytical difractometer. MOMENTO - Revista de Física; núm. 48E (2014); 38-51 0121-4470 .
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.spa.fl_str_mv application/pdf
dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia, Bogotá
institution Universidad Nacional de Colombia
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repository.name.fl_str_mv Repositorio Institucional Universidad Nacional de Colombia
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