Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados

ilustraciones, fotografías, gráficas, tablas

Autores:
Higuera Pedraza, Santiago Fernando
Tipo de recurso:
Fecha de publicación:
2021
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
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oai:repositorio.unal.edu.co:unal/81332
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/81332
https://repositorio.unal.edu.co/
Palabra clave:
Palm-oil
Spices
Oils and fats, Edible
Aceite de palma
Especias
Aceites y grasas comestibles
Cristalización
Polimorfismo
Aceite de palma
Grasas
Fats
Fat crystallization
Bouillon
Polymorphism
Palm oil
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
id UNACIONAL2_2b88f2274d8ff40a4837dc84b7350cb4
oai_identifier_str oai:repositorio.unal.edu.co:unal/81332
network_acronym_str UNACIONAL2
network_name_str Universidad Nacional de Colombia
repository_id_str
dc.title.spa.fl_str_mv Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
dc.title.translated.eng.fl_str_mv Evaluation of the crystallization process of palm oil-derived fats as binding agents in bouillons
title Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
spellingShingle Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
Palm-oil
Spices
Oils and fats, Edible
Aceite de palma
Especias
Aceites y grasas comestibles
Cristalización
Polimorfismo
Aceite de palma
Grasas
Fats
Fat crystallization
Bouillon
Polymorphism
Palm oil
title_short Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
title_full Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
title_fullStr Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
title_full_unstemmed Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
title_sort Evaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensados
dc.creator.fl_str_mv Higuera Pedraza, Santiago Fernando
dc.contributor.advisor.spa.fl_str_mv Fuenmayor Bobadilla, Carlos Alberto
Guitérrez Álvarez, Luis Felipe
dc.contributor.author.spa.fl_str_mv Higuera Pedraza, Santiago Fernando
dc.subject.lemb.eng.fl_str_mv Palm-oil
Spices
Oils and fats, Edible
topic Palm-oil
Spices
Oils and fats, Edible
Aceite de palma
Especias
Aceites y grasas comestibles
Cristalización
Polimorfismo
Aceite de palma
Grasas
Fats
Fat crystallization
Bouillon
Polymorphism
Palm oil
dc.subject.lemb.spa.fl_str_mv Aceite de palma
Especias
Aceites y grasas comestibles
dc.subject.proposal.spa.fl_str_mv Cristalización
Polimorfismo
Aceite de palma
Grasas
dc.subject.proposal.eng.fl_str_mv Fats
Fat crystallization
Bouillon
Polymorphism
Palm oil
description ilustraciones, fotografías, gráficas, tablas
publishDate 2021
dc.date.issued.none.fl_str_mv 2021-10-15
dc.date.accessioned.none.fl_str_mv 2022-03-23T19:18:17Z
dc.date.available.none.fl_str_mv 2022-03-23T19:18:17Z
dc.type.spa.fl_str_mv Trabajo de grado - Maestría
dc.type.driver.spa.fl_str_mv info:eu-repo/semantics/masterThesis
dc.type.version.spa.fl_str_mv info:eu-repo/semantics/acceptedVersion
dc.type.content.spa.fl_str_mv Text
dc.type.redcol.spa.fl_str_mv http://purl.org/redcol/resource_type/TM
status_str acceptedVersion
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/81332
dc.identifier.instname.spa.fl_str_mv Universidad Nacional de Colombia
dc.identifier.reponame.spa.fl_str_mv Repositorio Institucional Universidad Nacional de Colombia
dc.identifier.repourl.spa.fl_str_mv https://repositorio.unal.edu.co/
url https://repositorio.unal.edu.co/handle/unal/81332
https://repositorio.unal.edu.co/
identifier_str_mv Universidad Nacional de Colombia
Repositorio Institucional Universidad Nacional de Colombia
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.references.spa.fl_str_mv Afoakwa, Emmanuel Ohene, Alistair Paterson, Mark Fowler, and Joselio Vieira. 2008. “Effects of Tempering and Fat Crystallisation Behaviour on Microstructure, Mechanical Properties and Appearance in Dark Chocolate Systems.” Journal of Food Engineering 89 (2): 128–36. https://doi.org/10.1016/j.jfoodeng.2008.04.021.
Alander, Jari, Ann- Charlotte Anderson, Catharina Bagge, Karin Bringsarve, Monika Hjorth, and Martin Johansson. 2007. “Handbook: Vegetable Oils and Fats.”
Ariffin, A. 1994. Selected Readings on Palm Oil and Its Uses. Kuala Lumpur, Malaysia: Palm Oil Research Institute of Malaysia.
Barbosa-Cánovas, Gustavo V, Enrique Ortega-Rivas, Pablo Juliano, and Hong Yan. 2005. Food Powders. Food Powders. Food Engineering Series. https://doi.org/10.1007/0-387-27613-0.
Berger, K.G. 1975. “Uses of Palm Oil in the Food Industry.” Chemical Industry, 910.
Boistelle, R. 1988. “Fundamentals of Nucleation and Crystal Growth.” In Crystallization and Polymorphism of Fats and Fatty Acids. New: Mar.
Bongers, A. Gupta y P. 2011. “Bouillon Cube Process Design by Applying Product Druven Process Synthesis.” Chemical Engineering and Processing: Process Intensification, 9–15.
Brunello, Nadia, Sara E McGauley, and Alejandro Marangoni. 2003. “Mechanical Properties of Cocoa Butter in Relation to Its Crystallization Behavior and Microstructure.” LWT - Food Science and Technology 36 (5): 525–32. https://doi.org/https://doi.org/10.1016/S0023-6438(03)00053-7.
D’Souza, V., J. M. deMan, and L. deMan. 1990. “Short Spacings and Polymorphic Forms of Natural and Commercial Solid Fats: A Review.” Journal of the American Oil Chemists’ Society 67 (11): 835–43. https://doi.org/10.1007/BF02540502.
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dc.format.extent.spa.fl_str_mv xvii, 93 páginas
dc.format.mimetype.spa.fl_str_mv application/pdf
dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia
dc.publisher.program.spa.fl_str_mv Bogotá - Ciencias Agrarias - Maestría en Ciencia y Tecnología de Alimentos
dc.publisher.department.spa.fl_str_mv Instituto de Ciencia y Tecnología de Alimentos (ICTA)
dc.publisher.faculty.spa.fl_str_mv Facultad de Ciencias Agrarias
dc.publisher.place.spa.fl_str_mv Bogotá, Colombia
dc.publisher.branch.spa.fl_str_mv Universidad Nacional de Colombia - Sede Bogotá
institution Universidad Nacional de Colombia
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spelling Atribución-NoComercial 4.0 Internacionalhttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Fuenmayor Bobadilla, Carlos Alberto744ac643a2abaf4839cf342a0bc879a2600Guitérrez Álvarez, Luis Felipe84919393ea4baeac098b691ca4abe6c0Higuera Pedraza, Santiago Fernando58fc2584976540efc107979ddea7fe0f2022-03-23T19:18:17Z2022-03-23T19:18:17Z2021-10-15https://repositorio.unal.edu.co/handle/unal/81332Universidad Nacional de ColombiaRepositorio Institucional Universidad Nacional de Colombiahttps://repositorio.unal.edu.co/ilustraciones, fotografías, gráficas, tablasSe evaluó el proceso de cristalización de dos grasas derivadas del aceite de palma con diferentes puntos de fusión, durante el proceso de maduración, a -15°C, 4°C y 20°C por 12 horas, de una formulación de sazonador en polvo prensado, así como su efecto en las propiedades fisicoquímicas de humedad, factor de flujo y textura, y facilidad de uso por parte de consumidores. El proceso de cristalización fue estudiado por medio de las técnicas de calorimetría diferencial de barrido (DSC) y difracción de rayos X (XRD). La humedad fue medida por medio de una balanza infrarrojo y el factor de flujo mediante el instrumento Powder Flow Tester (PFT). Las propiedades de textura fueron evaluadas utilizando un analizador de textura y a través de un panel de desmenuzabilidad con 30 consumidores. Se logró evidenciar que la temperatura de maduración afecta el factor de flujo (ffc) de los sazonadores formados manteniendo su clasificación como polvos cohesivos (2<ffc<4) mientras que eliminando la grasa el sazonador pasa a ser altamente cohesivo (ffc>2) a las temperaturas de 4°C y 20°C de maduración. Por otro lado, la humedad de las muestras no se vio significativamente afectada (p>0.05) por la temperatura de maduración, pero si resultó ser significativamente mayor (p<0.05) en comparación con la muestra sin grasa para las tres temperaturas de maduración. Se lograron identificar principalmente cristales tipo β´ en las grasas, y cambios en su morfología durante la interacción con el sazonador. Comparativamente, se obtuvieron tabletas de menor dureza y más fáciles de desmenuzar con la grasa de menor punto de fusión a la menor temperatura de maduración (-15°C). Si bien este comportamiento se verificó en las tabletas elaboradas a escala piloto, en el proceso a escala industrial la diferencia en la facilidad de desmenuzar para los consumidores no fue significativa, subrayando la importancia de validar estos procesos en condiciones reales de producción. Estos resultados son de interés para la industria de caldos, puesto que establece las condiciones adecuadas para la etapa de maduración, crucial en la obtención de productos de alta calidad para los consumidores, y permite seguir avanzando en la investigación de matrices reales y sus componentes. (Texto tomado de la fuente).Crystallization process of two fats derived from palm oil with difference in their melting point during the maturation, at -15°C, 4°C and 20°C for 12 hours, of a standard bouillon formulation as its effect on the physical and chemical properties as relative humidity, flow factor, texture and consumer use easiness were evaluated. Crystal formation was studied by differential scanning calorimetry (DSC) and x ray diffraction (XRD) techniques. Relative humidity was measured by a halogen moisture analyzer and flow factor by the Powder Flow Tester. Texture properties were evaluated using a texture analyzer and with a 30 consumer crumbliness sensory evaluation. Results showed that maturation temperature affects the flow factor (ffc) of the bouillons maintaining its classification as cohesive powders (2<ffc<4) while eliminating any fat from the formula turns the classification into a highly cohesive powder (ffc<2) at 4°C and 20”C maturation temperatures. On the other hand, samples humidity was not significantly affected (p>0.05) by maturation temperature but it was significantly higher (p<0.05) compared with the free fat sample for the three maturation temperatures evaluated. β´ crystals in the fat samples and changes in their morphology due to interaction with bouillon components were identified. In contrast, softer and easier to crumble bouillon cubes formed were obtained with the least melting point fat at the coldest maturation temperature (-15°C). Although this behavior could be verified with the cubes formed pilot scale, in the industrial process the crumbliness evaluated by consumers was not significantly different between samples highlighting the importance of validating this process at real production conditions. These results are of interest for the bouillon industry while it establishes adequate conditions for the maturation stage, highly important for obtaining superior quality products and allows for advancing in the investigation of real foods and their components.MaestríaMagíster en Ciencia y Tecnología de AlimentosDiseño y desarrollo de productos alimenticiosxvii, 93 páginasapplication/pdfspaUniversidad Nacional de ColombiaBogotá - Ciencias Agrarias - Maestría en Ciencia y Tecnología de AlimentosInstituto de Ciencia y Tecnología de Alimentos (ICTA)Facultad de Ciencias AgrariasBogotá, ColombiaUniversidad Nacional de Colombia - Sede BogotáEvaluación de la cristalización de grasas derivadas de aceite de palma como agentes aglutinantes en sazonadores en polvo prensadosEvaluation of the crystallization process of palm oil-derived fats as binding agents in bouillonsTrabajo de grado - Maestríainfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/acceptedVersionTexthttp://purl.org/redcol/resource_type/TMAfoakwa, Emmanuel Ohene, Alistair Paterson, Mark Fowler, and Joselio Vieira. 2008. “Effects of Tempering and Fat Crystallisation Behaviour on Microstructure, Mechanical Properties and Appearance in Dark Chocolate Systems.” Journal of Food Engineering 89 (2): 128–36. https://doi.org/10.1016/j.jfoodeng.2008.04.021.Alander, Jari, Ann- Charlotte Anderson, Catharina Bagge, Karin Bringsarve, Monika Hjorth, and Martin Johansson. 2007. “Handbook: Vegetable Oils and Fats.”Ariffin, A. 1994. Selected Readings on Palm Oil and Its Uses. Kuala Lumpur, Malaysia: Palm Oil Research Institute of Malaysia.Barbosa-Cánovas, Gustavo V, Enrique Ortega-Rivas, Pablo Juliano, and Hong Yan. 2005. Food Powders. Food Powders. Food Engineering Series. https://doi.org/10.1007/0-387-27613-0.Berger, K.G. 1975. “Uses of Palm Oil in the Food Industry.” Chemical Industry, 910.Boistelle, R. 1988. “Fundamentals of Nucleation and Crystal Growth.” In Crystallization and Polymorphism of Fats and Fatty Acids. New: Mar.Bongers, A. Gupta y P. 2011. “Bouillon Cube Process Design by Applying Product Druven Process Synthesis.” Chemical Engineering and Processing: Process Intensification, 9–15.Brunello, Nadia, Sara E McGauley, and Alejandro Marangoni. 2003. “Mechanical Properties of Cocoa Butter in Relation to Its Crystallization Behavior and Microstructure.” LWT - Food Science and Technology 36 (5): 525–32. https://doi.org/https://doi.org/10.1016/S0023-6438(03)00053-7.D’Souza, V., J. 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New York, NY: Marcel Dekker, Inc.West, Ryan, and Dérick Rousseau. 2016. “Crystallization and Rheology of Palm Oil in the Presence of Sugar.” Food Research International 85 (July): 224–34. https://doi.org/10.1016/j.foodres.2016.05.010.Palm-oilSpicesOils and fats, EdibleAceite de palmaEspeciasAceites y grasas comestiblesCristalizaciónPolimorfismoAceite de palmaGrasasFatsFat crystallizationBouillonPolymorphismPalm oilInvestigadoresORIGINAL1032468200.2021.pdf1032468200.2021.pdfTesis de Maestría en Ciencia y Tecnología de Alimentosapplication/pdf1144355https://repositorio.unal.edu.co/bitstream/unal/81332/3/1032468200.2021.pdf900650b913bc16185e3c5735137b5446MD53LICENSElicense.txtlicense.txttext/plain; charset=utf-84074https://repositorio.unal.edu.co/bitstream/unal/81332/4/license.txt8153f7789df02f0a4c9e079953658ab2MD54THUMBNAIL1032468200.2021.pdf.jpg1032468200.2021.pdf.jpgGenerated 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