An easy method to prepare d3 and c2-tatp crystals

D3 and C2 TATP structures interconvert at room temperature. Herein, an easy method to isolate both conformers is shown that consists of multiple recrystallization steps using different solvent and heating to boiling. Spectroscopic and physical measurements, such as Raman spectroscopy, X-ray diffract...

Full description

Autores:

Espinosa Fuentes, Eduardo Antonio
Colpas Castillo, Fredy
Meza Fuentes, Edgardo
Ropero, Jorge

Tipo de recurso:

Article of journal

Fecha de publicación:

2016

Institución:

Corporación Universidad de la Costa

Repositorio:

REDICUC - Repositorio CUC

Idioma:

eng

OAI Identifier:

oai:repositorio.cuc.edu.co:11323/4211

Acceso en línea:

https://hdl.handle.net/11323/4211
https://repositorio.cuc.edu.co/

Palabra clave:

D3 and C2 TATP conformers
Raman
X-ray diffractogram
D3 y C2 conformadores TATP.
Raman
Difractograma de rayos x

Rights

openAccess

License

Attribution-NonCommercial-ShareAlike 4.0 International