Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix

This study investigates the properties of a composite material obtained by mixing Fe78Si9B13 metallic powders (at %) with graphene nanoplates (GNP) in an epoxy matrix. Four composite types were created with GNP weight proportions of 0%, 0.5%, 1.0%, and 1.5%. The composites were embedded in transpare...

Full description

Autores:
Pagnola, Marcelo Rubén
Faig, Javier
Ferrari, Sergio
Martinez Garcia, Ricardo
Useche Vivero, Jairo Francisco
Tipo de recurso:
Article of journal
Fecha de publicación:
2024
Institución:
Universidad Tecnológica de Bolívar
Repositorio:
Repositorio Institucional UTB
Idioma:
eng
OAI Identifier:
oai:repositorio.utb.edu.co:20.500.12585/13536
Acceso en línea:
https://hdl.handle.net/20.500.12585/13536
https://doi.org/10.32397/tesea.vol5.n1.593
Palabra clave:
Polvos Magnéticos
Nanoplacas de Grafeno
Composite
Deformación
Compresión
Modulo Elasticidad
Esfuerzos
Rights
openAccess
License
Marcelo Ruben Pagnola, Jairo Useche, Javier Faig, Sergio Ferrari, Ricardo Martinez Garcia - 2024
id UTB2_619279fae86261a44b17f88810b705bc
oai_identifier_str oai:repositorio.utb.edu.co:20.500.12585/13536
network_acronym_str UTB2
network_name_str Repositorio Institucional UTB
repository_id_str
dc.title.spa.fl_str_mv Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
dc.title.translated.spa.fl_str_mv Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
title Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
spellingShingle Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
Polvos Magnéticos
Nanoplacas de Grafeno
Composite
Deformación
Compresión
Modulo Elasticidad
Esfuerzos
title_short Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
title_full Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
title_fullStr Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
title_full_unstemmed Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
title_sort Study of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrix
dc.creator.fl_str_mv Pagnola, Marcelo Rubén
Faig, Javier
Ferrari, Sergio
Martinez Garcia, Ricardo
Useche Vivero, Jairo Francisco
dc.contributor.author.eng.fl_str_mv Pagnola, Marcelo Rubén
Faig, Javier
Ferrari, Sergio
Martinez Garcia, Ricardo
dc.contributor.author.none.fl_str_mv Useche Vivero, Jairo Francisco
dc.subject.eng.fl_str_mv Polvos Magnéticos
Nanoplacas de Grafeno
Composite
Deformación
Compresión
Modulo Elasticidad
Esfuerzos
topic Polvos Magnéticos
Nanoplacas de Grafeno
Composite
Deformación
Compresión
Modulo Elasticidad
Esfuerzos
description This study investigates the properties of a composite material obtained by mixing Fe78Si9B13 metallic powders (at %) with graphene nanoplates (GNP) in an epoxy matrix. Four composite types were created with GNP weight proportions of 0%, 0.5%, 1.0%, and 1.5%. The composites were embedded in transparent epoxy with weight proportions of 10%, 15%, and 20%, and then filled into 7 x 20 mm cylindrical probes. Twelve samples were prepared, and another 12 samples were subjected to a longitudinal magnetic field of 1 kG. All samples were tested with a Universal Testing Machine (Model WDW 10E) up to a maximum force of 20 kN. The experiment recorded deformation (ΔH) vs. charge force. Most samples showed a maximum compression resistance of 390 MPa, except for a few that did not exceed 100 MPa. The magnetically oriented samples showed a greater elastic limit in the range of 200 to 270 MPa. Optical microscopy was used to observe the ordering of the particles after the application of the magnetic field. Scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction were used to characterize the structure of the composite components. A vibrating sample magnetometer (VSM) was used to characterize the magnetic behavior of the metallic powders in the composite.
publishDate 2024
dc.date.accessioned.none.fl_str_mv 2024-06-30 11:55:40
2025-05-21T19:15:50Z
dc.date.available.none.fl_str_mv 2024-06-30 11:55:40
dc.date.issued.none.fl_str_mv 2024-06-30
dc.type.spa.fl_str_mv Artículo de revista
dc.type.coar.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
dc.type.driver.eng.fl_str_mv info:eu-repo/semantics/article
dc.type.coar.eng.fl_str_mv http://purl.org/coar/resource_type/c_6501
dc.type.local.eng.fl_str_mv Journal article
dc.type.content.eng.fl_str_mv Text
dc.type.version.eng.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.coarversion.eng.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a85
format http://purl.org/coar/resource_type/c_6501
status_str publishedVersion
dc.identifier.uri.none.fl_str_mv https://hdl.handle.net/20.500.12585/13536
dc.identifier.url.none.fl_str_mv https://doi.org/10.32397/tesea.vol5.n1.593
dc.identifier.doi.none.fl_str_mv 10.32397/tesea.vol5.n1.593
dc.identifier.eissn.none.fl_str_mv 2745-0120
url https://hdl.handle.net/20.500.12585/13536
https://doi.org/10.32397/tesea.vol5.n1.593
identifier_str_mv 10.32397/tesea.vol5.n1.593
2745-0120
dc.language.iso.eng.fl_str_mv eng
language eng
dc.relation.references.eng.fl_str_mv Fabiana Morales, Marcelo Pagnola, Juan Muriel, and Leandro Socolovsky. Molienda mecánica sobre cintas magnéticas blandas de fe78si9b13 con molino de bolas ortorrómbico de fabricación propia. Revista SAM N°1, page 61–67, 2020. [2] Da-guo Jiang and Zhao-hui Liu. Preparation and piezomagnetic effect of FeSiB amorphous powders /IIR composite film. In 2010 Third International Symposium on Intelligent Information Technology and Security Informatics, pages 268–270, 2010. [3] M. Pagnola, M. Malmoria, and M. Barone. Biot number behaviour in the chill block melt spinning (cbms) process. Applied Thermal Engineering, 103:807–811, 2016. [4] Marcelo R. Pagnola, Mariano Malmoria, Marcelo Barone, and Hugo Sirkin. Analysis of fe78si9b13 ( Multidiscipline Modeling in Materials and Structures, 10(4):511–524, Nov 2014. [5] N I C Berhanuddin, I Zaman, S A M Rozlan, M A A Karim, B Manshoor, A Khalid, S W Chan, and Q Meng. Enhancement of mechanical properties of epoxy/graphene nanocomposite. Journal of Physics: Conference Series, 914(1):012036, oct 2017. [6] M. R. Pagnola, F. Morales, P. Tancredi, and L. M. Socolovsky. Radial Distribution Function Analysis and Molecular Simulation of Graphene Nanoplatelets Obtained by Mechanical Ball Milling. JOM, 73(8):2471–2478, jan 2 2021. Transactions on Energy Systems and Engineering Applications, 5(1): 593, 2024 12 of 12 [7] MA Wenshi, Zhou Junwen, and Cheng Shunxi. Preparation and characterization of graphene. Journal of Chemical Engineering of Chinese Universities, 24(4):719–722, 2010. [8] J. Kováˇcik and Š. Emmer. Cross property connection between the electric and the thermal conductivities of copper graphite composites. International Journal of Engineering Science, 144:103130, 11 2019. [9] M. Pagnola, J. Useche V., and R. Martinez García. Obtención de Fe78Si9B13/GNPL composite: Un estudio de propiedades. 21st LACCEI International Multi-Conference for Engineering, Education, and Technology, (Buenos Aires, Argentina)., jul 18 2023. [10] I. Y. Jeon, Y. R. Shin, G. J. Sohn, H. J. Choi, S. Y. Bae, J. Mahmood, S. M. Jung, J. M. Seo, M. J. Kim, D. Wook Chang, L. Dai, and J. B. Baek. Edge-carboxylated graphene nanosheets via ball milling. Proceedings of the National Academy of Sciences, 109(15):5588–5593, mar 27 2012. [11] D14 Committee et al. Test method for apparent shear strength of single-lap-joint adhesively bonded metal specimens by tension loading (metal-to-metal). ASTM International, 2019. [12] Y. Dong, Z. Li, M. Liu, C. Chang, F. Li, and X. M. Wang. The effects of field annealing on the magnetic properties of FeSiB amorphous powder cores. Materials Research Bulletin, 96:160–163, 12 2017. [13] MC MORRIS, HF MCMURDIE, EH EVANS, B PARETZKIN, HS PARKER, NP PYRROS, and C HUBBARD. Standard x-ray diffraction power patterns: Section 20- data for 71 substances[final report]. 1984. [14] J. Zhang and F. Guyot. Thermal equation of state of iron and Fe0.91Si0.09. Physics and Chemistry of Minerals, 26(3):206–211, 1999. [15] CR Hubbard. Standard x-ray diffraction powder patterns: section 18—data for 58 substances. National Bureau of Standards Monogr, 1981. [16] G. Huang, C. Lv, J. He, X. Zhang, C. Zhou, P. Yang, Y. Tan, and H. Huang. Study on Preparation and Characterization of Graphene Based on Ball Milling Method. Journal of Nanomaterials, 2020:1–11, 2020.
dc.relation.ispartofjournal.eng.fl_str_mv Transactions on Energy Systems and Engineering Applications
dc.relation.citationvolume.eng.fl_str_mv 5
dc.relation.citationstartpage.none.fl_str_mv 1
dc.relation.citationendpage.none.fl_str_mv 12
dc.relation.bitstream.none.fl_str_mv https://revistas.utb.edu.co/tesea/article/download/593/393
dc.relation.citationedition.eng.fl_str_mv Núm. 1 , Año 2024 : Transactions on Energy Systems and Engineering Applications
dc.relation.citationissue.eng.fl_str_mv 1
dc.rights.eng.fl_str_mv Marcelo Ruben Pagnola, Jairo Useche, Javier Faig, Sergio Ferrari, Ricardo Martinez Garcia - 2024
dc.rights.uri.eng.fl_str_mv https://creativecommons.org/licenses/by/4.0
dc.rights.accessrights.eng.fl_str_mv info:eu-repo/semantics/openAccess
dc.rights.creativecommons.eng.fl_str_mv This work is licensed under a Creative Commons Attribution 4.0 International License.
dc.rights.coar.eng.fl_str_mv http://purl.org/coar/access_right/c_abf2
rights_invalid_str_mv Marcelo Ruben Pagnola, Jairo Useche, Javier Faig, Sergio Ferrari, Ricardo Martinez Garcia - 2024
https://creativecommons.org/licenses/by/4.0
This work is licensed under a Creative Commons Attribution 4.0 International License.
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.eng.fl_str_mv application/pdf
dc.publisher.eng.fl_str_mv Universidad Tecnológica de Bolívar
dc.source.eng.fl_str_mv https://revistas.utb.edu.co/tesea/article/view/593
institution Universidad Tecnológica de Bolívar
repository.name.fl_str_mv Repositorio Digital Universidad Tecnológica de Bolívar
repository.mail.fl_str_mv bdigital@metabiblioteca.com
_version_ 1858228433196154880
spelling Pagnola, Marcelo RubénFaig, JavierFerrari, SergioMartinez Garcia, RicardoUseche Vivero, Jairo Franciscovirtual::5226-12024-06-30 11:55:402025-05-21T19:15:50Z2024-06-30 11:55:402024-06-30https://hdl.handle.net/20.500.12585/13536https://doi.org/10.32397/tesea.vol5.n1.59310.32397/tesea.vol5.n1.5932745-0120This study investigates the properties of a composite material obtained by mixing Fe78Si9B13 metallic powders (at %) with graphene nanoplates (GNP) in an epoxy matrix. Four composite types were created with GNP weight proportions of 0%, 0.5%, 1.0%, and 1.5%. The composites were embedded in transparent epoxy with weight proportions of 10%, 15%, and 20%, and then filled into 7 x 20 mm cylindrical probes. Twelve samples were prepared, and another 12 samples were subjected to a longitudinal magnetic field of 1 kG. All samples were tested with a Universal Testing Machine (Model WDW 10E) up to a maximum force of 20 kN. The experiment recorded deformation (ΔH) vs. charge force. Most samples showed a maximum compression resistance of 390 MPa, except for a few that did not exceed 100 MPa. The magnetically oriented samples showed a greater elastic limit in the range of 200 to 270 MPa. Optical microscopy was used to observe the ordering of the particles after the application of the magnetic field. Scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction were used to characterize the structure of the composite components. A vibrating sample magnetometer (VSM) was used to characterize the magnetic behavior of the metallic powders in the composite.application/pdfengUniversidad Tecnológica de BolívarMarcelo Ruben Pagnola, Jairo Useche, Javier Faig, Sergio Ferrari, Ricardo Martinez Garcia - 2024https://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessThis work is licensed under a Creative Commons Attribution 4.0 International License.http://purl.org/coar/access_right/c_abf2https://revistas.utb.edu.co/tesea/article/view/593Polvos MagnéticosNanoplacas de GrafenoCompositeDeformaciónCompresiónModulo ElasticidadEsfuerzosStudy of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrixStudy of the properties of a composite material Fe78Si9B13 / GNP in an epoxy matrixArtículo de revistainfo:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1Journal articleTextinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/version/c_970fb48d4fbd8a85Fabiana Morales, Marcelo Pagnola, Juan Muriel, and Leandro Socolovsky. Molienda mecánica sobre cintas magnéticas blandas de fe78si9b13 con molino de bolas ortorrómbico de fabricación propia. Revista SAM N°1, page 61–67, 2020. [2] Da-guo Jiang and Zhao-hui Liu. Preparation and piezomagnetic effect of FeSiB amorphous powders /IIR composite film. In 2010 Third International Symposium on Intelligent Information Technology and Security Informatics, pages 268–270, 2010. [3] M. Pagnola, M. Malmoria, and M. Barone. Biot number behaviour in the chill block melt spinning (cbms) process. Applied Thermal Engineering, 103:807–811, 2016. [4] Marcelo R. Pagnola, Mariano Malmoria, Marcelo Barone, and Hugo Sirkin. Analysis of fe78si9b13 ( Multidiscipline Modeling in Materials and Structures, 10(4):511–524, Nov 2014. [5] N I C Berhanuddin, I Zaman, S A M Rozlan, M A A Karim, B Manshoor, A Khalid, S W Chan, and Q Meng. Enhancement of mechanical properties of epoxy/graphene nanocomposite. Journal of Physics: Conference Series, 914(1):012036, oct 2017. [6] M. R. Pagnola, F. Morales, P. Tancredi, and L. M. Socolovsky. Radial Distribution Function Analysis and Molecular Simulation of Graphene Nanoplatelets Obtained by Mechanical Ball Milling. JOM, 73(8):2471–2478, jan 2 2021. Transactions on Energy Systems and Engineering Applications, 5(1): 593, 2024 12 of 12 [7] MA Wenshi, Zhou Junwen, and Cheng Shunxi. Preparation and characterization of graphene. Journal of Chemical Engineering of Chinese Universities, 24(4):719–722, 2010. [8] J. Kováˇcik and Š. Emmer. Cross property connection between the electric and the thermal conductivities of copper graphite composites. International Journal of Engineering Science, 144:103130, 11 2019. [9] M. Pagnola, J. Useche V., and R. Martinez García. Obtención de Fe78Si9B13/GNPL composite: Un estudio de propiedades. 21st LACCEI International Multi-Conference for Engineering, Education, and Technology, (Buenos Aires, Argentina)., jul 18 2023. [10] I. Y. Jeon, Y. R. Shin, G. J. Sohn, H. J. Choi, S. Y. Bae, J. Mahmood, S. M. Jung, J. M. Seo, M. J. Kim, D. Wook Chang, L. Dai, and J. B. Baek. Edge-carboxylated graphene nanosheets via ball milling. Proceedings of the National Academy of Sciences, 109(15):5588–5593, mar 27 2012. [11] D14 Committee et al. Test method for apparent shear strength of single-lap-joint adhesively bonded metal specimens by tension loading (metal-to-metal). ASTM International, 2019. [12] Y. Dong, Z. Li, M. Liu, C. Chang, F. Li, and X. M. Wang. The effects of field annealing on the magnetic properties of FeSiB amorphous powder cores. Materials Research Bulletin, 96:160–163, 12 2017. [13] MC MORRIS, HF MCMURDIE, EH EVANS, B PARETZKIN, HS PARKER, NP PYRROS, and C HUBBARD. Standard x-ray diffraction power patterns: Section 20- data for 71 substances[final report]. 1984. [14] J. Zhang and F. Guyot. Thermal equation of state of iron and Fe0.91Si0.09. Physics and Chemistry of Minerals, 26(3):206–211, 1999. [15] CR Hubbard. Standard x-ray diffraction powder patterns: section 18—data for 58 substances. National Bureau of Standards Monogr, 1981. [16] G. Huang, C. Lv, J. He, X. Zhang, C. Zhou, P. Yang, Y. Tan, and H. Huang. Study on Preparation and Characterization of Graphene Based on Ball Milling Method. Journal of Nanomaterials, 2020:1–11, 2020.Transactions on Energy Systems and Engineering Applications5112https://revistas.utb.edu.co/tesea/article/download/593/393Núm. 1 , Año 2024 : Transactions on Energy Systems and Engineering Applications1Publication650842d2-583f-4e5a-92aa-2985c42d9ed8virtual::5226-1650842d2-583f-4e5a-92aa-2985c42d9ed8virtual::5226-120.500.12585/13536oai:repositorio.utb.edu.co:20.500.12585/135362025-06-24 14:40:41.359https://creativecommons.org/licenses/by/4.0Marcelo Ruben Pagnola, Jairo Useche, Javier Faig, Sergio Ferrari, Ricardo Martinez Garcia - 2024metadata.onlyhttps://repositorio.utb.edu.coRepositorio Digital Universidad Tecnológica de Bolívarbdigital@metabiblioteca.com

Publicaciones similares