Chromatographic analysis of phytochemicals in the peel of Musa paradisiaca to synthesize silver nanoparticles

This research work usedMusa paradisiaca(banana) peels as a natural solvent,assorted with the precursorAgNO3(10 mM) to perform the green synthesis of silvernanoparticles. The phytochemical components present in theMusa paradisiacapeelextracts were determined by gas chromatography coupled to a mass sp...

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Autores:
Buendia-Otero, María José
Tipo de recurso:
Fecha de publicación:
2020
Institución:
Universidad del Atlántico
Repositorio:
Repositorio Uniatlantico
Idioma:
eng
OAI Identifier:
oai:repositorio.uniatlantico.edu.co:20.500.12834/1129
Acceso en línea:
https://hdl.handle.net/20.500.12834/1129
https://www.scopus.com/record/display.uri?eid=2-s2.0-85120965653&doi=10.17533%2fudea.redin.20210427&origin=inward&txGid=f4d8548dd6aa6a06cb1d627b5d15d6e3
Palabra clave:
biosynthesis
nanoparticles
musa paradisiaca
chromatographic analysis
Rights
openAccess
License
http://creativecommons.org/licenses/by-nc/4.0/
Description
Summary:This research work usedMusa paradisiaca(banana) peels as a natural solvent,assorted with the precursorAgNO3(10 mM) to perform the green synthesis of silvernanoparticles. The phytochemical components present in theMusa paradisiacapeelextracts were determined by gas chromatography coupled to a mass spectrometer(GC-MS), and it was possible to identify the compounds: 1.2 Ethanediol (60.0261%) and 2.3 Butanediol (11.2 %); these -diols represent a highly reducing agent formetals, since they act as a solvent for the metal precursor behaving as a reducingagent, and facilitating the formation of nanoparticles. Likewise, the synthesized silvernanoparticles were subjected to a washing and drying treatment to be subsequentlycharacterized by means of UV-Vis and XRD techniques, resulting in a wavelength of411 nm, which is characteristic of these metallic nanoparticles, and achieving theidentification of the face-centered cubic structure (fcc) of the metallic silver, with anaverage particle size of 21.8 nm according to the Debye-Scherrer equation.