Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux

In this work shortcut methods are developed for the conceptual design of azeotropic and extractive distillation. Three specific cases of azeotropic and extractive distillation are studied: single-feed homogeneous azeotropic distillation, extractive homogeneous distillation and single-feed heterogene...

Full description

Autores:
Estupiñan Pérez, Libardo
Tipo de recurso:
Fecha de publicación:
2012
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/19993
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/19993
http://bdigital.unal.edu.co/10217/
Palabra clave:
51 Matemáticas / Mathematics
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Reversible distillation
Distillation boundaries
Finite reflux
Operation leaves
Continuation methods
Conceptual design
Azeotropic distillation
Destilación reversible
Fronteras de destilación
Reflujo finito
Hojas de operación
Métodos de continuación
Diseño conceptual
Destilación azeotrópica
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
id UNACIONAL2_eea22de0629b9a6527a0fe8d6b84fe54
oai_identifier_str oai:repositorio.unal.edu.co:unal/19993
network_acronym_str UNACIONAL2
network_name_str Universidad Nacional de Colombia
repository_id_str
dc.title.spa.fl_str_mv Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
title Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
spellingShingle Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
51 Matemáticas / Mathematics
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Reversible distillation
Distillation boundaries
Finite reflux
Operation leaves
Continuation methods
Conceptual design
Azeotropic distillation
Destilación reversible
Fronteras de destilación
Reflujo finito
Hojas de operación
Métodos de continuación
Diseño conceptual
Destilación azeotrópica
title_short Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
title_full Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
title_fullStr Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
title_full_unstemmed Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
title_sort Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux
dc.creator.fl_str_mv Estupiñan Pérez, Libardo
dc.contributor.author.spa.fl_str_mv Estupiñan Pérez, Libardo
dc.contributor.spa.fl_str_mv Martínez Riascos, Carlos Arturo
dc.subject.ddc.spa.fl_str_mv 51 Matemáticas / Mathematics
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
topic 51 Matemáticas / Mathematics
66 Ingeniería química y Tecnologías relacionadas/ Chemical engineering
Reversible distillation
Distillation boundaries
Finite reflux
Operation leaves
Continuation methods
Conceptual design
Azeotropic distillation
Destilación reversible
Fronteras de destilación
Reflujo finito
Hojas de operación
Métodos de continuación
Diseño conceptual
Destilación azeotrópica
dc.subject.proposal.spa.fl_str_mv Reversible distillation
Distillation boundaries
Finite reflux
Operation leaves
Continuation methods
Conceptual design
Azeotropic distillation
Destilación reversible
Fronteras de destilación
Reflujo finito
Hojas de operación
Métodos de continuación
Diseño conceptual
Destilación azeotrópica
description In this work shortcut methods are developed for the conceptual design of azeotropic and extractive distillation. Three specific cases of azeotropic and extractive distillation are studied: single-feed homogeneous azeotropic distillation, extractive homogeneous distillation and single-feed heterogeneous distillation. To evaluate the process feasibility, to calculate design parameters and minimum energy by shortcut methods is the core of this work. Methods developed are based on the pinch concept and the use of mathematical tools for modeling the thermodynamic behavior. Continuation methods are used throughout the work in order to either devise or modify calculation algorithms that can be robust and useful for any kind of mixture. Finally, different mixtures with academic or industrial relevance were selected as case studies to demonstrate the applicability of conceptual design and shortcut methods in distillation process. Obtained results demonstrate that the use of conceptual design methods is an efficient way to avoid the trial and error design strategy carried out in simulators by engineers.
publishDate 2012
dc.date.issued.spa.fl_str_mv 2012
dc.date.accessioned.spa.fl_str_mv 2019-06-25T18:22:09Z
dc.date.available.spa.fl_str_mv 2019-06-25T18:22:09Z
dc.type.spa.fl_str_mv Trabajo de grado - Maestría
dc.type.driver.spa.fl_str_mv info:eu-repo/semantics/masterThesis
dc.type.version.spa.fl_str_mv info:eu-repo/semantics/acceptedVersion
dc.type.content.spa.fl_str_mv Text
dc.type.redcol.spa.fl_str_mv http://purl.org/redcol/resource_type/TM
status_str acceptedVersion
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/19993
dc.identifier.eprints.spa.fl_str_mv http://bdigital.unal.edu.co/10217/
url https://repositorio.unal.edu.co/handle/unal/19993
http://bdigital.unal.edu.co/10217/
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Sede Bogotá Facultad de Ingeniería Departamento de Ingeniería Química y Ambiental
Departamento de Ingeniería Química y Ambiental
dc.relation.references.spa.fl_str_mv Estupiñan Pérez, Libardo (2012) Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux. Maestría thesis, Universidad Nacional de Colombia.
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.spa.fl_str_mv application/pdf
institution Universidad Nacional de Colombia
bitstream.url.fl_str_mv https://repositorio.unal.edu.co/bitstream/unal/19993/1/300434.2012.pdf
https://repositorio.unal.edu.co/bitstream/unal/19993/2/300434.2012.pdf.jpg
bitstream.checksum.fl_str_mv 8665866769e9d0a2151b0f92e9bd3567
bc3fbd8e802094814409c6bf5571f395
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositorio Institucional Universidad Nacional de Colombia
repository.mail.fl_str_mv repositorio_nal@unal.edu.co
_version_ 1814089880083365888
spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Martínez Riascos, Carlos ArturoEstupiñan Pérez, Libardo59cbf7a9-1036-465f-b66f-95d78fe8f52c3002019-06-25T18:22:09Z2019-06-25T18:22:09Z2012https://repositorio.unal.edu.co/handle/unal/19993http://bdigital.unal.edu.co/10217/In this work shortcut methods are developed for the conceptual design of azeotropic and extractive distillation. Three specific cases of azeotropic and extractive distillation are studied: single-feed homogeneous azeotropic distillation, extractive homogeneous distillation and single-feed heterogeneous distillation. To evaluate the process feasibility, to calculate design parameters and minimum energy by shortcut methods is the core of this work. Methods developed are based on the pinch concept and the use of mathematical tools for modeling the thermodynamic behavior. Continuation methods are used throughout the work in order to either devise or modify calculation algorithms that can be robust and useful for any kind of mixture. Finally, different mixtures with academic or industrial relevance were selected as case studies to demonstrate the applicability of conceptual design and shortcut methods in distillation process. Obtained results demonstrate that the use of conceptual design methods is an efficient way to avoid the trial and error design strategy carried out in simulators by engineers.En este trabajo métodos cortos fueron desarrollados para el diseño conceptual de la destilación extractiva y azeotrópica. Tres diferentes casos de destilación azeotrópica y extractiva fueron estudiados: destilación azeotrópica homogénea en columnas con un alimento, destilación extractiva homogénea y destilación heterogénea en columnas con un alimento. La evaluación de la factibilidad del proceso, el cálculo de los parámetros de diseño y la mínima energía constituyen el núcleo del presente trabajo. Los métodos desarrollados están basados en el concepto del pinchy el uso de herramientas matemáticas para modelar el comportamiento termodinámico. Métodos de continuación son usados a lo largo del trabajo ya sea para el desarrollo o para modificar algoritmos de cálculo que sean robustos y aplicables a cualquier clase de mezcla. Finalmente, diferentes mezclas con relevancia académica o industrial fueron seleccionadas como casos de estudio para demostrar la aplicabilidad del diseño conceptual y los métodos cortos en el proceso de destilación. Los resultados obtenidos demuestran que el uso de los métodos cortos en el diseño conceptual son una forma eficiente para evitar el diseño mediante una estrategia de ensayo y error usando simuladores comerciales.Maestríaapplication/pdfspaUniversidad Nacional de Colombia Sede Bogotá Facultad de Ingeniería Departamento de Ingeniería Química y AmbientalDepartamento de Ingeniería Química y AmbientalEstupiñan Pérez, Libardo (2012) Tools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite reflux. Maestría thesis, Universidad Nacional de Colombia.51 Matemáticas / Mathematics66 Ingeniería química y Tecnologías relacionadas/ Chemical engineeringReversible distillationDistillation boundariesFinite refluxOperation leavesContinuation methodsConceptual designAzeotropic distillationDestilación reversibleFronteras de destilaciónReflujo finitoHojas de operaciónMétodos de continuaciónDiseño conceptualDestilación azeotrópicaTools development for analysis and conceptual design of extractive and azeotropic distillation columns at finite refluxTrabajo de grado - Maestríainfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/acceptedVersionTexthttp://purl.org/redcol/resource_type/TMORIGINAL300434.2012.pdfapplication/pdf3113400https://repositorio.unal.edu.co/bitstream/unal/19993/1/300434.2012.pdf8665866769e9d0a2151b0f92e9bd3567MD51THUMBNAIL300434.2012.pdf.jpg300434.2012.pdf.jpgGenerated Thumbnailimage/jpeg4647https://repositorio.unal.edu.co/bitstream/unal/19993/2/300434.2012.pdf.jpgbc3fbd8e802094814409c6bf5571f395MD52unal/19993oai:repositorio.unal.edu.co:unal/199932022-11-02 16:05:46.201Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co

Publicaciones similares