Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template

Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterize...

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Autores:
Buitrago-Vásquez, Maritza
Ossa-Orozco, Claudia Patricia
Tipo de recurso:
Article of journal
Fecha de publicación:
2018
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/68556
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/68556
http://bdigital.unal.edu.co/69589/
Palabra clave:
62 Ingeniería y operaciones afines / Engineering
hydroxyapatite
bioceramics
nanorods
hydrothermal reaction
fruit extract template
hidroxiapatita
biocerámicos
nanobarras
síntesis hidrotermal
plantilla de extracto de fruta
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
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oai_identifier_str oai:repositorio.unal.edu.co:unal/68556
network_acronym_str UNACIONAL2
network_name_str Universidad Nacional de Colombia
repository_id_str
spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Buitrago-Vásquez, Maritza05e9001f-6fb2-4cc6-beca-a61851d27645300Ossa-Orozco, Claudia Patricia1b4640eb-335a-46c9-9c20-3da17ba8266d3002019-07-03T07:07:10Z2019-07-03T07:07:10Z2018-01-01ISSN: 2346-2183https://repositorio.unal.edu.co/handle/unal/68556http://bdigital.unal.edu.co/69589/Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterized using a hydrothermal reaction with templates of fruit extracts in order to control the particles size and morphology. The powders obtained were characterized by scanning electron microscopy, X-ray diffraction, and infrared spectroscopy. Hydroxyapatite nanorods were obtained with diameters between 43.47 and 48.56 nm and lengths between 148.47 and 265.96 nm. For all assays, an adequate HA synthesis was confirmed because the XRD showed the main and secondary peaks. The crystallite size was calculated with the Scherrer equation, obtaining values between 5.99 and 6.96 nm and percentages crystallinity between 55.61 and 65.9%. The synthesized material can be a suitable biomaterial for the manufacture of bone substitutes.El desarrollo de biomateriales para el reemplazo de partes del cuerpo humano ha sido una de las necesidades de la ciencia. La hidroxiapatita es un biocerámico similar al componente mineral de los tejidos duros del cuerpo humano y animal. En la presente investigación se sintetizaron nanobarras de hidroxiapatita usando síntesis hidrotermal con plantillas de extractos de fruta para controlar el tamaño de partícula, los polvos obtenidos se caracterizaron por microscopia electrónica de barrido, difracción de rayos x y espectroscopia infrarroja. Las nanobarras obtenidas presentaron diámetros entre 43,47 y 48,56 nm, longitudes entre 148,47 y 265,96 nm, para todos los ensayos los DRX mostraron los picos principales y secundarios de la hidroxiapatita. El tamaño del cristalito fue calculado con la ecuación de Scherrer con valores entre 5,99 y 6,96 nm y porcentajes de cristalinidad entre 55,61 y 65,9%. En conclusión el material sintetizado puede usarse como biomaterial para aplicaciones óseas.application/pdfspaUniversidad Nacional de Colombia - Sede Medellín - Facultad de Minashttps://revistas.unal.edu.co/index.php/dyna/article/view/65773Universidad Nacional de Colombia Revistas electrónicas UN DynaDynaBuitrago-Vásquez, Maritza and Ossa-Orozco, Claudia Patricia (2018) Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template. DYNA, 85 (204). pp. 283-288. ISSN 2346-218362 Ingeniería y operaciones afines / Engineeringhydroxyapatitebioceramicsnanorodshydrothermal reactionfruit extract templatehidroxiapatitabiocerámicosnanobarrassíntesis hidrotermalplantilla de extracto de frutaHydrothermal synthesis of hydroxyapatite nanorods using a fruit extract templateArtículo de revistainfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1http://purl.org/coar/version/c_970fb48d4fbd8a85Texthttp://purl.org/redcol/resource_type/ARTORIGINAL65773-376696-3-PB.pdfapplication/pdf767846https://repositorio.unal.edu.co/bitstream/unal/68556/1/65773-376696-3-PB.pdfef185dfde29e5fb2c0b221f107e9f8c8MD51THUMBNAIL65773-376696-3-PB.pdf.jpg65773-376696-3-PB.pdf.jpgGenerated Thumbnailimage/jpeg9516https://repositorio.unal.edu.co/bitstream/unal/68556/2/65773-376696-3-PB.pdf.jpgb44f5ff88f91245ff6b97b899872c5dbMD52unal/68556oai:repositorio.unal.edu.co:unal/685562024-05-27 23:09:33.968Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co
dc.title.spa.fl_str_mv Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
spellingShingle Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
62 Ingeniería y operaciones afines / Engineering
hydroxyapatite
bioceramics
nanorods
hydrothermal reaction
fruit extract template
hidroxiapatita
biocerámicos
nanobarras
síntesis hidrotermal
plantilla de extracto de fruta
title_short Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_full Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_fullStr Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_full_unstemmed Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_sort Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
dc.creator.fl_str_mv Buitrago-Vásquez, Maritza
Ossa-Orozco, Claudia Patricia
dc.contributor.author.spa.fl_str_mv Buitrago-Vásquez, Maritza
Ossa-Orozco, Claudia Patricia
dc.subject.ddc.spa.fl_str_mv 62 Ingeniería y operaciones afines / Engineering
topic 62 Ingeniería y operaciones afines / Engineering
hydroxyapatite
bioceramics
nanorods
hydrothermal reaction
fruit extract template
hidroxiapatita
biocerámicos
nanobarras
síntesis hidrotermal
plantilla de extracto de fruta
dc.subject.proposal.spa.fl_str_mv hydroxyapatite
bioceramics
nanorods
hydrothermal reaction
fruit extract template
hidroxiapatita
biocerámicos
nanobarras
síntesis hidrotermal
plantilla de extracto de fruta
description Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterized using a hydrothermal reaction with templates of fruit extracts in order to control the particles size and morphology. The powders obtained were characterized by scanning electron microscopy, X-ray diffraction, and infrared spectroscopy. Hydroxyapatite nanorods were obtained with diameters between 43.47 and 48.56 nm and lengths between 148.47 and 265.96 nm. For all assays, an adequate HA synthesis was confirmed because the XRD showed the main and secondary peaks. The crystallite size was calculated with the Scherrer equation, obtaining values between 5.99 and 6.96 nm and percentages crystallinity between 55.61 and 65.9%. The synthesized material can be a suitable biomaterial for the manufacture of bone substitutes.
publishDate 2018
dc.date.issued.spa.fl_str_mv 2018-01-01
dc.date.accessioned.spa.fl_str_mv 2019-07-03T07:07:10Z
dc.date.available.spa.fl_str_mv 2019-07-03T07:07:10Z
dc.type.spa.fl_str_mv Artículo de revista
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dc.type.content.spa.fl_str_mv Text
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format http://purl.org/coar/resource_type/c_6501
status_str publishedVersion
dc.identifier.issn.spa.fl_str_mv ISSN: 2346-2183
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/68556
dc.identifier.eprints.spa.fl_str_mv http://bdigital.unal.edu.co/69589/
identifier_str_mv ISSN: 2346-2183
url https://repositorio.unal.edu.co/handle/unal/68556
http://bdigital.unal.edu.co/69589/
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.spa.fl_str_mv https://revistas.unal.edu.co/index.php/dyna/article/view/65773
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Revistas electrónicas UN Dyna
Dyna
dc.relation.references.spa.fl_str_mv Buitrago-Vásquez, Maritza and Ossa-Orozco, Claudia Patricia (2018) Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template. DYNA, 85 (204). pp. 283-288. ISSN 2346-2183
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.spa.fl_str_mv application/pdf
dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia - Sede Medellín - Facultad de Minas
institution Universidad Nacional de Colombia
bitstream.url.fl_str_mv https://repositorio.unal.edu.co/bitstream/unal/68556/1/65773-376696-3-PB.pdf
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