Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study

The synthesis and characterization of different N-phenyl-N-(1-phenylhex-5-en-1-yl)acetamides is presented. Two conformational isomers were observed for one of the compounds in their1H/13C-NMR spectra. Computational calculations and dihedral angle comparison using the allylic system coupling constant...

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Autores:
Acelas, Mauricio
Gil, Elizabeth
Doerr, Markus
Daza, Martha
Urbina, Juan Manuel
Tipo de recurso:
Article of journal
Fecha de publicación:
2013
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/49112
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/49112
http://bdigital.unal.edu.co/42569/
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Atribución-NoComercial 4.0 Internacional
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spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Acelas, Mauriciofde4b459-802d-410e-94a3-56dbb686d81f300Gil, Elizabeth61a9cba1-db17-4d89-ba73-2db93b291691300Doerr, Markusec6fa543-e809-4869-8006-39b6e4856dc8300Daza, Martha1b3476b2-0122-4cb5-92f1-275d9c77c497300Urbina, Juan Manuel3fc6ceb9-51c4-47a5-8c1e-df610c5cfbc83002019-06-29T08:24:22Z2019-06-29T08:24:22Z2013https://repositorio.unal.edu.co/handle/unal/49112http://bdigital.unal.edu.co/42569/The synthesis and characterization of different N-phenyl-N-(1-phenylhex-5-en-1-yl)acetamides is presented. Two conformational isomers were observed for one of the compounds in their1H/13C-NMR spectra. Computational calculations and dihedral angle comparison using the allylic system coupling constants (J) were carried out to determine the isomeric structures responsible for signals duplicity and chemical shifting.application/pdfspaUniversidad Nacional de Colombiahttp://revistas.unal.edu.co/index.php/rcolquim/article/view/44404Universidad Nacional de Colombia Revistas electrónicas UN Revista Colombiana de QuímicaRevista Colombiana de QuímicaRevista Colombiana de Química; Vol. 42, núm. 1 (2013) 2357-3791 0120-2804Acelas, Mauricio and Gil, Elizabeth and Doerr, Markus and Daza, Martha and Urbina, Juan Manuel (2013) Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study. Revista Colombiana de Química; Vol. 42, núm. 1 (2013) 2357-3791 0120-2804 .Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational studyArtículo de revistainfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1http://purl.org/coar/version/c_970fb48d4fbd8a85Texthttp://purl.org/redcol/resource_type/ARTORIGINAL44404-209740-1-PB.pdfapplication/pdf1343859https://repositorio.unal.edu.co/bitstream/unal/49112/1/44404-209740-1-PB.pdf17e9c5c6005e8c74830a3b870973a389MD51THUMBNAIL44404-209740-1-PB.pdf.jpg44404-209740-1-PB.pdf.jpgGenerated Thumbnailimage/jpeg8035https://repositorio.unal.edu.co/bitstream/unal/49112/2/44404-209740-1-PB.pdf.jpg69aece792a7bda86e66bbbdea50dc389MD52unal/49112oai:repositorio.unal.edu.co:unal/491122022-11-14 23:02:44.372Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co
dc.title.spa.fl_str_mv Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
spellingShingle Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title_short Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title_full Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title_fullStr Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title_full_unstemmed Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
title_sort Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study
dc.creator.fl_str_mv Acelas, Mauricio
Gil, Elizabeth
Doerr, Markus
Daza, Martha
Urbina, Juan Manuel
dc.contributor.author.spa.fl_str_mv Acelas, Mauricio
Gil, Elizabeth
Doerr, Markus
Daza, Martha
Urbina, Juan Manuel
description The synthesis and characterization of different N-phenyl-N-(1-phenylhex-5-en-1-yl)acetamides is presented. Two conformational isomers were observed for one of the compounds in their1H/13C-NMR spectra. Computational calculations and dihedral angle comparison using the allylic system coupling constants (J) were carried out to determine the isomeric structures responsible for signals duplicity and chemical shifting.
publishDate 2013
dc.date.issued.spa.fl_str_mv 2013
dc.date.accessioned.spa.fl_str_mv 2019-06-29T08:24:22Z
dc.date.available.spa.fl_str_mv 2019-06-29T08:24:22Z
dc.type.spa.fl_str_mv Artículo de revista
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http://bdigital.unal.edu.co/42569/
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dc.relation.spa.fl_str_mv http://revistas.unal.edu.co/index.php/rcolquim/article/view/44404
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Revistas electrónicas UN Revista Colombiana de Química
Revista Colombiana de Química
dc.relation.ispartofseries.none.fl_str_mv Revista Colombiana de Química; Vol. 42, núm. 1 (2013) 2357-3791 0120-2804
dc.relation.references.spa.fl_str_mv Acelas, Mauricio and Gil, Elizabeth and Doerr, Markus and Daza, Martha and Urbina, Juan Manuel (2013) Synthesis of new n-phenyl-n-(1-phenylhex-5-en-1-yl)acetamides and their 1h-nmr conformational study. Revista Colombiana de Química; Vol. 42, núm. 1 (2013) 2357-3791 0120-2804 .
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
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dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia
institution Universidad Nacional de Colombia
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