Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production

Batch distillation applied to hydrous ethanol fuel (HEF) production on a small scale still requires operating conditions that ensure optimal top product quality and productivity. The aim of this study is to statistically validate a batch still through the employment of response surface methodology (...

Full description

Autores:
Foletto, Edson Luiz
Tipo de recurso:
Article of journal
Fecha de publicación:
2015
Institución:
Universidad Nacional de Colombia
Repositorio:
Universidad Nacional de Colombia
Idioma:
spa
OAI Identifier:
oai:repositorio.unal.edu.co:unal/67692
Acceso en línea:
https://repositorio.unal.edu.co/handle/unal/67692
http://bdigital.unal.edu.co/68721/
Palabra clave:
62 Ingeniería y operaciones afines / Engineering
Batch distillation
ethanol fuel
process optimization
factorial design
destilación diferencial
etanol combustible
optimización de procesos
diseño factorial
Rights
openAccess
License
Atribución-NoComercial 4.0 Internacional
id UNACIONAL2_26720ff6a78b38212aaf59493c37b4b0
oai_identifier_str oai:repositorio.unal.edu.co:unal/67692
network_acronym_str UNACIONAL2
network_name_str Universidad Nacional de Colombia
repository_id_str
dc.title.spa.fl_str_mv Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
title Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
spellingShingle Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
62 Ingeniería y operaciones afines / Engineering
Batch distillation
ethanol fuel
process optimization
factorial design
destilación diferencial
etanol combustible
optimización de procesos
diseño factorial
title_short Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
title_full Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
title_fullStr Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
title_full_unstemmed Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
title_sort Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production
dc.creator.fl_str_mv Foletto, Edson Luiz
dc.contributor.author.spa.fl_str_mv Foletto, Edson Luiz
dc.subject.ddc.spa.fl_str_mv 62 Ingeniería y operaciones afines / Engineering
topic 62 Ingeniería y operaciones afines / Engineering
Batch distillation
ethanol fuel
process optimization
factorial design
destilación diferencial
etanol combustible
optimización de procesos
diseño factorial
dc.subject.proposal.spa.fl_str_mv Batch distillation
ethanol fuel
process optimization
factorial design
destilación diferencial
etanol combustible
optimización de procesos
diseño factorial
description Batch distillation applied to hydrous ethanol fuel (HEF) production on a small scale still requires operating conditions that ensure optimal top product quality and productivity. The aim of this study is to statistically validate a batch still through the employment of response surface methodology (RSM). Operational and productivity parameters were formulated in order to guarantee quality compliance with the legal requirements for the top product concentration, besides providing support information to control the production of HEF on a small scale. The reboiler control and dephlegmator temperatures maintained within the range of 97.5 to 99.5°C and 60 to 70°C, respectively, combined with a variable reflux ratio, was satisfactory in obtaining a top product concentration, in accordance with legal regulations, as well as high productivity. The results of this study may contribute to the assembly of a simple and low-cost batch distillation control system.
publishDate 2015
dc.date.issued.spa.fl_str_mv 2015-01-01
dc.date.accessioned.spa.fl_str_mv 2019-07-03T04:52:23Z
dc.date.available.spa.fl_str_mv 2019-07-03T04:52:23Z
dc.type.spa.fl_str_mv Artículo de revista
dc.type.coar.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
dc.type.driver.spa.fl_str_mv info:eu-repo/semantics/article
dc.type.version.spa.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.coar.spa.fl_str_mv http://purl.org/coar/resource_type/c_6501
dc.type.coarversion.spa.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.content.spa.fl_str_mv Text
dc.type.redcol.spa.fl_str_mv http://purl.org/redcol/resource_type/ART
format http://purl.org/coar/resource_type/c_6501
status_str publishedVersion
dc.identifier.issn.spa.fl_str_mv ISSN: 2248-8723
dc.identifier.uri.none.fl_str_mv https://repositorio.unal.edu.co/handle/unal/67692
dc.identifier.eprints.spa.fl_str_mv http://bdigital.unal.edu.co/68721/
identifier_str_mv ISSN: 2248-8723
url https://repositorio.unal.edu.co/handle/unal/67692
http://bdigital.unal.edu.co/68721/
dc.language.iso.spa.fl_str_mv spa
language spa
dc.relation.spa.fl_str_mv https://revistas.unal.edu.co/index.php/ingeinv/article/view/46969
dc.relation.ispartof.spa.fl_str_mv Universidad Nacional de Colombia Revistas electrónicas UN Ingeniería e Investigación
Ingeniería e Investigación
dc.relation.references.spa.fl_str_mv Foletto, Edson Luiz (2015) Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production. Ingeniería e Investigación, 35 (1). pp. 31-35. ISSN 2248-8723
dc.rights.spa.fl_str_mv Derechos reservados - Universidad Nacional de Colombia
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.spa.fl_str_mv Atribución-NoComercial 4.0 Internacional
dc.rights.uri.spa.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.accessrights.spa.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv Atribución-NoComercial 4.0 Internacional
Derechos reservados - Universidad Nacional de Colombia
http://creativecommons.org/licenses/by-nc/4.0/
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.mimetype.spa.fl_str_mv application/pdf
dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia - Sede Bogotá - Facultad de Ingeniería
institution Universidad Nacional de Colombia
bitstream.url.fl_str_mv https://repositorio.unal.edu.co/bitstream/unal/67692/1/46969-244822-1-PB.pdf
https://repositorio.unal.edu.co/bitstream/unal/67692/2/46969-244822-1-PB.pdf.jpg
bitstream.checksum.fl_str_mv 2438ae29c3944930680d0baa97d11178
69a0c590ecb2779d9edf6c0a31df9e16
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositorio Institucional Universidad Nacional de Colombia
repository.mail.fl_str_mv repositorio_nal@unal.edu.co
_version_ 1814089507199254528
spelling Atribución-NoComercial 4.0 InternacionalDerechos reservados - Universidad Nacional de Colombiahttp://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Foletto, Edson Luiz1e992b6c-496a-4869-b0ae-d8a0e278a56f3002019-07-03T04:52:23Z2019-07-03T04:52:23Z2015-01-01ISSN: 2248-8723https://repositorio.unal.edu.co/handle/unal/67692http://bdigital.unal.edu.co/68721/Batch distillation applied to hydrous ethanol fuel (HEF) production on a small scale still requires operating conditions that ensure optimal top product quality and productivity. The aim of this study is to statistically validate a batch still through the employment of response surface methodology (RSM). Operational and productivity parameters were formulated in order to guarantee quality compliance with the legal requirements for the top product concentration, besides providing support information to control the production of HEF on a small scale. The reboiler control and dephlegmator temperatures maintained within the range of 97.5 to 99.5°C and 60 to 70°C, respectively, combined with a variable reflux ratio, was satisfactory in obtaining a top product concentration, in accordance with legal regulations, as well as high productivity. The results of this study may contribute to the assembly of a simple and low-cost batch distillation control system.La destilación diferencial aplicada a la producción de etanol hidratado combustible (EHC) a pequeña escala todavía requiere condiciones de operación que aseguren la calidad del producto destilado y la productividad óptimas. El objetivo de esta investigación es validar estadísticamente la destilación diferencial mediante el empleo de la metodología de superficie de respuesta (MSR). Parámetros operacionales y de productividad se han formulado con el objetivo de garantizar el cumplimiento de la calidad de los requisitos legales para la concentración del producto destilado, además de proporcionar información de apoyo para el control de la producción de EHC a pequeña escala. El control de las temperaturas del rehervidor y deflegmador, mantenidos dentro del intervalo de 97,5 a 99,5 °C y de 60 a 70°C, respectivamente, en combinación con una relación de reflujo variable fueron satisfactorios en la obtención de una concentración del producto destilado en conformidad con las normas legales, así como una alta productividad. Los resultados de este estudio pueden contribuir al montaje de un sistema de control de destilación diferencial simplificado y de bajo costo.application/pdfspaUniversidad Nacional de Colombia - Sede Bogotá - Facultad de Ingenieríahttps://revistas.unal.edu.co/index.php/ingeinv/article/view/46969Universidad Nacional de Colombia Revistas electrónicas UN Ingeniería e InvestigaciónIngeniería e InvestigaciónFoletto, Edson Luiz (2015) Operation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) production. Ingeniería e Investigación, 35 (1). pp. 31-35. ISSN 2248-872362 Ingeniería y operaciones afines / EngineeringBatch distillationethanol fuelprocess optimizationfactorial designdestilación diferencialetanol combustibleoptimización de procesosdiseño factorialOperation parameters of a small scale batch distillation column for hydrous ethanol fuel (HEF) productionArtículo de revistainfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1http://purl.org/coar/version/c_970fb48d4fbd8a85Texthttp://purl.org/redcol/resource_type/ARTORIGINAL46969-244822-1-PB.pdfapplication/pdf504384https://repositorio.unal.edu.co/bitstream/unal/67692/1/46969-244822-1-PB.pdf2438ae29c3944930680d0baa97d11178MD51THUMBNAIL46969-244822-1-PB.pdf.jpg46969-244822-1-PB.pdf.jpgGenerated Thumbnailimage/jpeg8887https://repositorio.unal.edu.co/bitstream/unal/67692/2/46969-244822-1-PB.pdf.jpg69a0c590ecb2779d9edf6c0a31df9e16MD52unal/67692oai:repositorio.unal.edu.co:unal/676922023-05-31 23:03:09.545Repositorio Institucional Universidad Nacional de Colombiarepositorio_nal@unal.edu.co