Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)

La búsqueda de nuevos materiales que puedan ser usados como pigmentos y que sean amigables con el medio ambiente ha llevado al estudio de una nueva familia YIn1-xMxO3 en la cual el sitio ocupado por el catión In3+ es sustituido por distintos metales de transición como el Mn3+, Fe3+ y Cu2+/Zr4+, dand...

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Autores:
Bravo Lopez, Mayerly Karina
Florez Mariño, Saul Andres
Tipo de recurso:
http://purl.org/coar/version/c_b1a7d7d4d402bcce
Fecha de publicación:
2016
Institución:
Universidad Industrial de Santander
Repositorio:
Repositorio UIS
Idioma:
spa
OAI Identifier:
oai:noesis.uis.edu.co:20.500.14071/34299
Acceso en línea:
https://noesis.uis.edu.co/handle/20.500.14071/34299
https://noesis.uis.edu.co
Palabra clave:
Pigmento Inorganico
Estructura Hexagonal
Sintesis Sol-Gel
Difraccion De Rayos X
Ciel*A*B*.
The search for new materials that can be used as pigments and are friendly to the environment has led to the study of a new family YIn1-xMxO3 in which the site occupied by the cation In3+ is replaced with various transition metals such as Mn3+
Fe3+ and Cu2+/Zr4+
giving as a result powder blue
yellow and green color respectively. The materials were prepared by the sol-gel method and citrate-nitrate
characterized by the technique of X-ray diffraction
the analysis showed the XRD patterns forming the desired hexagonal phase with the space group P63cm. The optical properties were studied by diffuse reflectance technique and from the spectra obtained the parameters L*a*b* were calculated from the space color CIELAB using the Optprop application from Matlab software. The stability study of materials was performed by exposing the powder samples to different means of common use which could expose the materials according to the future implementation
is also a water-based paint was prepared using the pigment manufactured
which he also performed a stability study using the same means as the powder samples. And finally they were again carried out to the XRD measurements and the diffuse reflectance to establish changes presented during each experiment
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Attribution-NonCommercial 4.0 International (CC BY-NC 4.0)
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network_acronym_str UISANTADR2
network_name_str Repositorio UIS
repository_id_str
dc.title.none.fl_str_mv Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
dc.title.english.none.fl_str_mv Inorganic Pigment, Hexagonal Structure, Sol-Gel Synthesis, X-Ray Powder Diffraction, Ciel*A*B*.
title Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
spellingShingle Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
Pigmento Inorganico
Estructura Hexagonal
Sintesis Sol-Gel
Difraccion De Rayos X
Ciel*A*B*.
The search for new materials that can be used as pigments and are friendly to the environment has led to the study of a new family YIn1-xMxO3 in which the site occupied by the cation In3+ is replaced with various transition metals such as Mn3+
Fe3+ and Cu2+/Zr4+
giving as a result powder blue
yellow and green color respectively. The materials were prepared by the sol-gel method and citrate-nitrate
characterized by the technique of X-ray diffraction
the analysis showed the XRD patterns forming the desired hexagonal phase with the space group P63cm. The optical properties were studied by diffuse reflectance technique and from the spectra obtained the parameters L*a*b* were calculated from the space color CIELAB using the Optprop application from Matlab software. The stability study of materials was performed by exposing the powder samples to different means of common use which could expose the materials according to the future implementation
is also a water-based paint was prepared using the pigment manufactured
which he also performed a stability study using the same means as the powder samples. And finally they were again carried out to the XRD measurements and the diffuse reflectance to establish changes presented during each experiment
title_short Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
title_full Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
title_fullStr Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
title_full_unstemmed Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
title_sort Síntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)
dc.creator.fl_str_mv Bravo Lopez, Mayerly Karina
Florez Mariño, Saul Andres
dc.contributor.advisor.none.fl_str_mv Gauthier, Gilles Henri
Macias Lopez, Mario Alberto
dc.contributor.author.none.fl_str_mv Bravo Lopez, Mayerly Karina
Florez Mariño, Saul Andres
dc.subject.none.fl_str_mv Pigmento Inorganico
Estructura Hexagonal
Sintesis Sol-Gel
Difraccion De Rayos X
Ciel*A*B*.
topic Pigmento Inorganico
Estructura Hexagonal
Sintesis Sol-Gel
Difraccion De Rayos X
Ciel*A*B*.
The search for new materials that can be used as pigments and are friendly to the environment has led to the study of a new family YIn1-xMxO3 in which the site occupied by the cation In3+ is replaced with various transition metals such as Mn3+
Fe3+ and Cu2+/Zr4+
giving as a result powder blue
yellow and green color respectively. The materials were prepared by the sol-gel method and citrate-nitrate
characterized by the technique of X-ray diffraction
the analysis showed the XRD patterns forming the desired hexagonal phase with the space group P63cm. The optical properties were studied by diffuse reflectance technique and from the spectra obtained the parameters L*a*b* were calculated from the space color CIELAB using the Optprop application from Matlab software. The stability study of materials was performed by exposing the powder samples to different means of common use which could expose the materials according to the future implementation
is also a water-based paint was prepared using the pigment manufactured
which he also performed a stability study using the same means as the powder samples. And finally they were again carried out to the XRD measurements and the diffuse reflectance to establish changes presented during each experiment
dc.subject.keyword.none.fl_str_mv The search for new materials that can be used as pigments and are friendly to the environment has led to the study of a new family YIn1-xMxO3 in which the site occupied by the cation In3+ is replaced with various transition metals such as Mn3+
Fe3+ and Cu2+/Zr4+
giving as a result powder blue
yellow and green color respectively. The materials were prepared by the sol-gel method and citrate-nitrate
characterized by the technique of X-ray diffraction
the analysis showed the XRD patterns forming the desired hexagonal phase with the space group P63cm. The optical properties were studied by diffuse reflectance technique and from the spectra obtained the parameters L*a*b* were calculated from the space color CIELAB using the Optprop application from Matlab software. The stability study of materials was performed by exposing the powder samples to different means of common use which could expose the materials according to the future implementation
is also a water-based paint was prepared using the pigment manufactured
which he also performed a stability study using the same means as the powder samples. And finally they were again carried out to the XRD measurements and the diffuse reflectance to establish changes presented during each experiment
description La búsqueda de nuevos materiales que puedan ser usados como pigmentos y que sean amigables con el medio ambiente ha llevado al estudio de una nueva familia YIn1-xMxO3 en la cual el sitio ocupado por el catión In3+ es sustituido por distintos metales de transición como el Mn3+, Fe3+ y Cu2+/Zr4+, dando como resultado polvos de color azul, amarillo y verde respectivamente. Los materiales fueron preparados por el método sol-gel citrato-nitrato y caracterizados mediante la técnica de difracción de rayos X. El análisis de los patrones de DRX mostró la formación de la fase hexagonal deseada con grupo espacial P63cm. Las propiedades ópticas se estudiaron por medio de la técnica de reflectancia difusa y a partir de los espectros obtenidos se calcularon los parámetros L*a*b* del espacio del color CIELAB usando la aplicación Optprop del software de Matlab. El estudio de estabilidad de los materiales se realizó por medio de la exposición de muestras en polvo a diferentes medios de uso común a los cuales podrían exponerse los materiales de acuerdo a una aplicación futura, además se elaboró una pintura de base acuosa empleando el pigmento fabricado, a la cual también se le realizó un estudio de estabilidad empleando los mismos medios que las muestras en polvo. Y finalmente se realizaron nuevamente las mediciones de DRX y reflectancia difusa para establecer cambios presentados durante cada experimentación
publishDate 2016
dc.date.available.none.fl_str_mv 2016
2024-03-03T22:36:44Z
dc.date.created.none.fl_str_mv 2016
dc.date.issued.none.fl_str_mv 2016
dc.date.accessioned.none.fl_str_mv 2024-03-03T22:36:44Z
dc.type.local.none.fl_str_mv Tesis/Trabajo de grado - Monografía - Pregrado
dc.type.hasversion.none.fl_str_mv http://purl.org/coar/resource_type/c_7a1f
dc.type.coar.none.fl_str_mv http://purl.org/coar/version/c_b1a7d7d4d402bcce
format http://purl.org/coar/version/c_b1a7d7d4d402bcce
dc.identifier.uri.none.fl_str_mv https://noesis.uis.edu.co/handle/20.500.14071/34299
dc.identifier.instname.none.fl_str_mv Universidad Industrial de Santander
dc.identifier.reponame.none.fl_str_mv Universidad Industrial de Santander
dc.identifier.repourl.none.fl_str_mv https://noesis.uis.edu.co
url https://noesis.uis.edu.co/handle/20.500.14071/34299
https://noesis.uis.edu.co
identifier_str_mv Universidad Industrial de Santander
dc.language.iso.none.fl_str_mv spa
language spa
dc.rights.none.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.license.none.fl_str_mv Attribution-NonCommercial 4.0 International (CC BY-NC 4.0)
dc.rights.uri.none.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0
dc.rights.creativecommons.none.fl_str_mv Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)
rights_invalid_str_mv Attribution-NonCommercial 4.0 International (CC BY-NC 4.0)
http://creativecommons.org/licenses/by/4.0/
http://creativecommons.org/licenses/by-nc/4.0
Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)
http://purl.org/coar/access_right/c_abf2
dc.format.mimetype.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidad Industrial de Santander
dc.publisher.faculty.none.fl_str_mv Facultad de Ingenierías Fisicoquímicas
dc.publisher.program.none.fl_str_mv Ingeniería Química
dc.publisher.school.none.fl_str_mv Escuela de Ingeniería Química
publisher.none.fl_str_mv Universidad Industrial de Santander
institution Universidad Industrial de Santander
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spelling Attribution-NonCommercial 4.0 International (CC BY-NC 4.0)http://creativecommons.org/licenses/by/4.0/http://creativecommons.org/licenses/by-nc/4.0Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)http://purl.org/coar/access_right/c_abf2Gauthier, Gilles HenriMacias Lopez, Mario AlbertoBravo Lopez, Mayerly KarinaFlorez Mariño, Saul Andres2024-03-03T22:36:44Z20162024-03-03T22:36:44Z20162016https://noesis.uis.edu.co/handle/20.500.14071/34299Universidad Industrial de SantanderUniversidad Industrial de Santanderhttps://noesis.uis.edu.coLa búsqueda de nuevos materiales que puedan ser usados como pigmentos y que sean amigables con el medio ambiente ha llevado al estudio de una nueva familia YIn1-xMxO3 en la cual el sitio ocupado por el catión In3+ es sustituido por distintos metales de transición como el Mn3+, Fe3+ y Cu2+/Zr4+, dando como resultado polvos de color azul, amarillo y verde respectivamente. Los materiales fueron preparados por el método sol-gel citrato-nitrato y caracterizados mediante la técnica de difracción de rayos X. El análisis de los patrones de DRX mostró la formación de la fase hexagonal deseada con grupo espacial P63cm. Las propiedades ópticas se estudiaron por medio de la técnica de reflectancia difusa y a partir de los espectros obtenidos se calcularon los parámetros L*a*b* del espacio del color CIELAB usando la aplicación Optprop del software de Matlab. El estudio de estabilidad de los materiales se realizó por medio de la exposición de muestras en polvo a diferentes medios de uso común a los cuales podrían exponerse los materiales de acuerdo a una aplicación futura, además se elaboró una pintura de base acuosa empleando el pigmento fabricado, a la cual también se le realizó un estudio de estabilidad empleando los mismos medios que las muestras en polvo. Y finalmente se realizaron nuevamente las mediciones de DRX y reflectancia difusa para establecer cambios presentados durante cada experimentaciónPregradoIngeniero QuímicoSynthesis and stability study of pigments (y,zr)(in,m)o3 (m=mn, fe, cu)application/pdfspaUniversidad Industrial de SantanderFacultad de Ingenierías FisicoquímicasIngeniería QuímicaEscuela de Ingeniería QuímicaPigmento InorganicoEstructura HexagonalSintesis Sol-GelDifraccion De Rayos XCiel*A*B*.The search for new materials that can be used as pigments and are friendly to the environment has led to the study of a new family YIn1-xMxO3 in which the site occupied by the cation In3+ is replaced with various transition metals such as Mn3+Fe3+ and Cu2+/Zr4+giving as a result powder blueyellow and green color respectively. The materials were prepared by the sol-gel method and citrate-nitratecharacterized by the technique of X-ray diffractionthe analysis showed the XRD patterns forming the desired hexagonal phase with the space group P63cm. The optical properties were studied by diffuse reflectance technique and from the spectra obtained the parameters L*a*b* were calculated from the space color CIELAB using the Optprop application from Matlab software. The stability study of materials was performed by exposing the powder samples to different means of common use which could expose the materials according to the future implementationis also a water-based paint was prepared using the pigment manufacturedwhich he also performed a stability study using the same means as the powder samples. And finally they were again carried out to the XRD measurements and the diffuse reflectance to establish changes presented during each experimentSíntesis y estudio de estabilidad de pigmentos (y,zr)(in,m)o3(m=mn, fe, cu)Inorganic Pigment, Hexagonal Structure, Sol-Gel Synthesis, X-Ray Powder Diffraction, Ciel*A*B*.Tesis/Trabajo de grado - Monografía - Pregradohttp://purl.org/coar/resource_type/c_7a1fhttp://purl.org/coar/version/c_b1a7d7d4d402bcceORIGINALCarta de autorización.pdfapplication/pdf351487https://noesis.uis.edu.co/bitstreams/04c38d1b-f963-4bd5-b18c-082e05f0f88e/downloadc6727e59f70262132622397027d4565eMD51Documento.pdfapplication/pdf2954528https://noesis.uis.edu.co/bitstreams/0622c7c8-46b7-47e6-b691-466f44f04742/download694ff02ac34953b3b0272101380fbc5bMD52Nota de proyecto.pdfapplication/pdf206108https://noesis.uis.edu.co/bitstreams/6852db64-e9d5-4650-85c3-9eba117be1a9/downloade279a129f2cf1a9eb623bea56aa4bce6MD5320.500.14071/34299oai:noesis.uis.edu.co:20.500.14071/342992024-03-03 17:36:44.077http://creativecommons.org/licenses/by-nc/4.0http://creativecommons.org/licenses/by/4.0/open.accesshttps://noesis.uis.edu.coDSpace at UISnoesis@uis.edu.co