Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling

ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained,...

Full description

Autores:
Ríos Arbeláez, Jesús María
Restrepo Carvajal, Alex Humberto
Zuleta Gil, Alejandro Alberto
Bolívar Osorio, Francisco Javier
Castaño González, Juan Guillermo
Correa Bedoya, Esteban Alberto
Echeverría Echeverría, Félix
Tipo de recurso:
Article of investigation
Fecha de publicación:
2021
Institución:
Universidad de Antioquia
Repositorio:
Repositorio UdeA
Idioma:
eng
OAI Identifier:
oai:bibliotecadigital.udea.edu.co:10495/23199
Acceso en línea:
http://hdl.handle.net/10495/23199
Palabra clave:
Microestructura
Microstructure
Recristalización (metalurgia)
Recrystallization (Metallurgy)
Milling parameters
Morphological changes
Magnesium powders
Rights
openAccess
License
http://creativecommons.org/licenses/by/2.5/co/
id UDEA2_bee28e9ac630794e5b98a13d6785b0e5
oai_identifier_str oai:bibliotecadigital.udea.edu.co:10495/23199
network_acronym_str UDEA2
network_name_str Repositorio UdeA
repository_id_str
dc.title.spa.fl_str_mv Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
title Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
spellingShingle Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
Microestructura
Microstructure
Recristalización (metalurgia)
Recrystallization (Metallurgy)
Milling parameters
Morphological changes
Magnesium powders
title_short Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
title_full Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
title_fullStr Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
title_full_unstemmed Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
title_sort Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
dc.creator.fl_str_mv Ríos Arbeláez, Jesús María
Restrepo Carvajal, Alex Humberto
Zuleta Gil, Alejandro Alberto
Bolívar Osorio, Francisco Javier
Castaño González, Juan Guillermo
Correa Bedoya, Esteban Alberto
Echeverría Echeverría, Félix
dc.contributor.author.none.fl_str_mv Ríos Arbeláez, Jesús María
Restrepo Carvajal, Alex Humberto
Zuleta Gil, Alejandro Alberto
Bolívar Osorio, Francisco Javier
Castaño González, Juan Guillermo
Correa Bedoya, Esteban Alberto
Echeverría Echeverría, Félix
dc.subject.lemb.none.fl_str_mv Microestructura
Microstructure
Recristalización (metalurgia)
Recrystallization (Metallurgy)
topic Microestructura
Microstructure
Recristalización (metalurgia)
Recrystallization (Metallurgy)
Milling parameters
Morphological changes
Magnesium powders
dc.subject.proposal.spa.fl_str_mv Milling parameters
Morphological changes
Magnesium powders
description ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained, it was determined that the ball size is the most influential milling parameter. This was because balls of 1 mm diameter were used after a previous stage of milling with larger balls (i.e., 10 and 3 mm). The powder particles presented an unusual morphology with respect to those observed in the Mg-milling literature and recrystallization phenomena. Moreover, the result strongly varied depending on the ball-to-powder weight ratio (BPR) used during the milling process.
publishDate 2021
dc.date.accessioned.none.fl_str_mv 2021-10-14T17:46:26Z
dc.date.available.none.fl_str_mv 2021-10-14T17:46:26Z
dc.date.issued.none.fl_str_mv 2021
dc.type.spa.fl_str_mv info:eu-repo/semantics/article
dc.type.coarversion.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.hasversion.spa.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.coar.spa.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
dc.type.redcol.spa.fl_str_mv https://purl.org/redcol/resource_type/ART
dc.type.local.spa.fl_str_mv Artículo de investigación
format http://purl.org/coar/resource_type/c_2df8fbb1
status_str publishedVersion
dc.identifier.citation.spa.fl_str_mv Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621
dc.identifier.uri.none.fl_str_mv http://hdl.handle.net/10495/23199
dc.identifier.doi.none.fl_str_mv 10.3390/met11101621
dc.identifier.eissn.none.fl_str_mv 2075-4701
identifier_str_mv Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621
10.3390/met11101621
2075-4701
url http://hdl.handle.net/10495/23199
dc.language.iso.spa.fl_str_mv eng
language eng
dc.relation.ispartofjournalabbrev.spa.fl_str_mv Metals
dc.rights.spa.fl_str_mv info:eu-repo/semantics/openAccess
dc.rights.uri.*.fl_str_mv http://creativecommons.org/licenses/by/2.5/co/
dc.rights.accessrights.spa.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.creativecommons.spa.fl_str_mv https://creativecommons.org/licenses/by/4.0/
eu_rights_str_mv openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by/2.5/co/
http://purl.org/coar/access_right/c_abf2
https://creativecommons.org/licenses/by/4.0/
dc.format.extent.spa.fl_str_mv 10
dc.format.mimetype.spa.fl_str_mv application/pdf
dc.publisher.spa.fl_str_mv MDPI
dc.publisher.group.spa.fl_str_mv Centro de Investigación Innovación y Desarrollo de Materiales (CIDEMAT)
dc.publisher.place.spa.fl_str_mv Basilea, Suiza
institution Universidad de Antioquia
bitstream.url.fl_str_mv http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/1/RiosJesus_2021_Effectball.pdf
http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/2/license_rdf
http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/3/license.txt
bitstream.checksum.fl_str_mv 68e6348277820f6f16f3d5ab02dd1a4f
1646d1f6b96dbbbc38035efc9239ac9c
8a4605be74aa9ea9d79846c1fba20a33
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
repository.name.fl_str_mv Repositorio Institucional Universidad de Antioquia
repository.mail.fl_str_mv andres.perez@udea.edu.co
_version_ 1805390245231853568
spelling Ríos Arbeláez, Jesús MaríaRestrepo Carvajal, Alex HumbertoZuleta Gil, Alejandro AlbertoBolívar Osorio, Francisco JavierCastaño González, Juan GuillermoCorrea Bedoya, Esteban AlbertoEcheverría Echeverría, Félix2021-10-14T17:46:26Z2021-10-14T17:46:26Z2021Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621http://hdl.handle.net/10495/2319910.3390/met111016212075-4701ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained, it was determined that the ball size is the most influential milling parameter. This was because balls of 1 mm diameter were used after a previous stage of milling with larger balls (i.e., 10 and 3 mm). The powder particles presented an unusual morphology with respect to those observed in the Mg-milling literature and recrystallization phenomena. Moreover, the result strongly varied depending on the ball-to-powder weight ratio (BPR) used during the milling process.COL00079271.329.112.20610application/pdfengMDPICentro de Investigación Innovación y Desarrollo de Materiales (CIDEMAT)Basilea, Suizainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_2df8fbb1https://purl.org/redcol/resource_type/ARTArtículo de investigaciónhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by/2.5/co/http://purl.org/coar/access_right/c_abf2https://creativecommons.org/licenses/by/4.0/Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball MillingMicroestructuraMicrostructureRecristalización (metalurgia)Recrystallization (Metallurgy)Milling parametersMorphological changesMagnesium powdersMetalsMetals1101110Departamento Administrativo de Ciencia, Tecnología e Innovación, MincienciasPrograma Nacional en IngenieríaObtención de nuevas aleaciones ligeras de alto valor agregado para contribuir al desarrollo de las industrias de biomateriales y aeronáuticas del país80740-183-2019ORIGINALRiosJesus_2021_Effectball.pdfRiosJesus_2021_Effectball.pdfArtículo de investigaciónapplication/pdf2118460http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/1/RiosJesus_2021_Effectball.pdf68e6348277820f6f16f3d5ab02dd1a4fMD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8927http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/2/license_rdf1646d1f6b96dbbbc38035efc9239ac9cMD52LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://bibliotecadigital.udea.edu.co/bitstream/10495/23199/3/license.txt8a4605be74aa9ea9d79846c1fba20a33MD5310495/23199oai:bibliotecadigital.udea.edu.co:10495/231992021-10-14 12:46:27.081Repositorio Institucional Universidad de Antioquiaandres.perez@udea.edu.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