Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template

ABSTRACT: Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and ch...

Full description

Autores:
Buitrago Vásquez, Maritza
Ossa Orozco, Claudia Patricia
Tipo de recurso:
Article of investigation
Fecha de publicación:
2018
Institución:
Universidad de Antioquia
Repositorio:
Repositorio UdeA
Idioma:
eng
OAI Identifier:
oai:bibliotecadigital.udea.edu.co:10495/23373
Acceso en línea:
http://hdl.handle.net/10495/23373
Palabra clave:
Materiales Biocompatibles
Biocompatible Materials
Nanotecnología
Nanotechnology
Hidroxiapatitas
Biocerámicos
Extracto de frutas
Rights
openAccess
License
http://creativecommons.org/licenses/by-nc-nd/2.5/co/
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oai_identifier_str oai:bibliotecadigital.udea.edu.co:10495/23373
network_acronym_str UDEA2
network_name_str Repositorio UdeA
repository_id_str
dc.title.spa.fl_str_mv Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
dc.title.alternative.spa.fl_str_mv Síntesis hidrotermal de nanobarras de hidroxiapatita usando plantillas de extractos de fruta
title Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
spellingShingle Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
Materiales Biocompatibles
Biocompatible Materials
Nanotecnología
Nanotechnology
Hidroxiapatitas
Biocerámicos
Extracto de frutas
title_short Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_full Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_fullStr Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_full_unstemmed Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
title_sort Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract template
dc.creator.fl_str_mv Buitrago Vásquez, Maritza
Ossa Orozco, Claudia Patricia
dc.contributor.author.none.fl_str_mv Buitrago Vásquez, Maritza
Ossa Orozco, Claudia Patricia
dc.subject.decs.none.fl_str_mv Materiales Biocompatibles
Biocompatible Materials
topic Materiales Biocompatibles
Biocompatible Materials
Nanotecnología
Nanotechnology
Hidroxiapatitas
Biocerámicos
Extracto de frutas
dc.subject.lemb.none.fl_str_mv Nanotecnología
Nanotechnology
dc.subject.proposal.spa.fl_str_mv Hidroxiapatitas
Biocerámicos
Extracto de frutas
description ABSTRACT: Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterized using a hydrothermal reaction with templates of fruit extracts in order to control the particles size and morphology. The powders obtained were characterized by scanning electron microscopy, X-ray diffraction, and infrared spectroscopy. Hydroxyapatite nanorods were obtained with diameters between 43.47 and 48.56 nm and lengths between 148.47 and 265.96 nm. For all assays, an adequate HA synthesis was confirmed because the XRD showed the main and secondary peaks. The crystallite size was calculated with the Scherrer equation, obtaining values between 5.99 and 6.96 nm and percentages crystallinity between 55.61 and 65.9%. The synthesized material can be a suitable biomaterial for the manufacture of bone substitutes.
publishDate 2018
dc.date.issued.none.fl_str_mv 2018
dc.date.accessioned.none.fl_str_mv 2021-10-22T02:06:54Z
dc.date.available.none.fl_str_mv 2021-10-22T02:06:54Z
dc.type.spa.fl_str_mv info:eu-repo/semantics/article
dc.type.coarversion.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.hasversion.spa.fl_str_mv info:eu-repo/semantics/publishedVersion
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dc.type.local.spa.fl_str_mv Artículo de investigación
format http://purl.org/coar/resource_type/c_2df8fbb1
status_str publishedVersion
dc.identifier.issn.none.fl_str_mv 0012-7353
dc.identifier.uri.none.fl_str_mv http://hdl.handle.net/10495/23373
dc.identifier.doi.none.fl_str_mv 10.15446/dyna.v85n204.65773
dc.identifier.eissn.none.fl_str_mv 2346-2183
identifier_str_mv 0012-7353
10.15446/dyna.v85n204.65773
2346-2183
url http://hdl.handle.net/10495/23373
dc.language.iso.spa.fl_str_mv eng
language eng
dc.relation.ispartofjournalabbrev.spa.fl_str_mv Dyna
dc.rights.spa.fl_str_mv info:eu-repo/semantics/openAccess
dc.rights.uri.*.fl_str_mv http://creativecommons.org/licenses/by-nc-nd/2.5/co/
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dc.format.extent.spa.fl_str_mv 6
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dc.publisher.spa.fl_str_mv Universidad Nacional de Colombia, Facultad de Minas, Centro de Publicaciones
dc.publisher.group.spa.fl_str_mv Grupo de Investigación en Biomateriales
dc.publisher.place.spa.fl_str_mv Medellín, Colombia
institution Universidad de Antioquia
bitstream.url.fl_str_mv http://bibliotecadigital.udea.edu.co/bitstream/10495/23373/3/license.txt
http://bibliotecadigital.udea.edu.co/bitstream/10495/23373/1/BuitragoMaritza_2018_HydrotermalHydroxyapatite.pdf
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spelling Buitrago Vásquez, MaritzaOssa Orozco, Claudia Patricia2021-10-22T02:06:54Z2021-10-22T02:06:54Z20180012-7353http://hdl.handle.net/10495/2337310.15446/dyna.v85n204.657732346-2183ABSTRACT: Biocompatible materials development for the replacement of human body parts has been one of the needs of science. Hydroxyapatite is a bioceramic similar to the mineral component present in the human hard tissues and animal body. In this work, hydroxyapatite nanorods were synthesized and characterized using a hydrothermal reaction with templates of fruit extracts in order to control the particles size and morphology. The powders obtained were characterized by scanning electron microscopy, X-ray diffraction, and infrared spectroscopy. Hydroxyapatite nanorods were obtained with diameters between 43.47 and 48.56 nm and lengths between 148.47 and 265.96 nm. For all assays, an adequate HA synthesis was confirmed because the XRD showed the main and secondary peaks. The crystallite size was calculated with the Scherrer equation, obtaining values between 5.99 and 6.96 nm and percentages crystallinity between 55.61 and 65.9%. The synthesized material can be a suitable biomaterial for the manufacture of bone substitutes.RESUMEN: El desarrollo de biomateriales para el reemplazo de partes del cuerpo humano ha sido una de las necesidades de la ciencia. La hidroxiapatita es un biocerámico similar al componente mineral de los tejidos duros del cuerpo humano y animal. En la presente investigación, se sintetizaron nanobarras de hidroxiapatita usando síntesis hidrotermal con plantillas de extractos de fruta para controlar el tamaño de partícula. Los polvos obtenidos se caracterizaron por microscopia electrónica de barrido, difracción de rayos x y espectroscopia infrarroja. Las nanobarras obtenidas presentaron diámetros entre 43,47 y 48,56 nm, longitudes entre 148,47 y 265,96 nm. para todos los ensayos los DRX mostraron los picos principales y secundarios de la hidroxiapatita. El tamaño del cristalito fue calculado con la ecuación de Scherrer con valores entre 5,99 y 6,96 nm. y porcentajes de cristalinidad entre 55,61 y 65,9%. En conclusión el material sintetizado puede usarse como biomaterial para aplicaciones óseas.COL00550496application/pdfengUniversidad Nacional de Colombia, Facultad de Minas, Centro de PublicacionesGrupo de Investigación en BiomaterialesMedellín, Colombiainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_2df8fbb1https://purl.org/redcol/resource_type/ARTArtículo de investigaciónhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-nd/2.5/co/http://purl.org/coar/access_right/c_abf2https://creativecommons.org/licenses/by-nc-nd/4.0/Hydrothermal synthesis of hydroxyapatite nanorods using a fruit extract templateSíntesis hidrotermal de nanobarras de hidroxiapatita usando plantillas de extractos de frutaMateriales BiocompatiblesBiocompatible MaterialsNanotecnologíaNanotechnologyHidroxiapatitasBiocerámicosExtracto de frutasDynaDyna28328885204LICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://bibliotecadigital.udea.edu.co/bitstream/10495/23373/3/license.txt8a4605be74aa9ea9d79846c1fba20a33MD53ORIGINALBuitragoMaritza_2018_HydrotermalHydroxyapatite.pdfBuitragoMaritza_2018_HydrotermalHydroxyapatite.pdfArtículo de investigaciónapplication/pdf767846http://bibliotecadigital.udea.edu.co/bitstream/10495/23373/1/BuitragoMaritza_2018_HydrotermalHydroxyapatite.pdfef185dfde29e5fb2c0b221f107e9f8c8MD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8823http://bibliotecadigital.udea.edu.co/bitstream/10495/23373/2/license_rdfb88b088d9957e670ce3b3fbe2eedbc13MD5210495/23373oai:bibliotecadigital.udea.edu.co:10495/233732021-10-21 21:30:15.318Repositorio Institucional Universidad de Antioquiaandres.perez@udea.edu.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