Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method
ABSTRACT: In this paper the synthesis of the LaBiFe2O6 material by the modified Pechini method is reported. Structural, morphologic, magnetic and optic experimental studies were performed. Rietveld refinement of x-ray diffraction patterns revealed that LaBiFe2O6 crystallizes in an orthorhombic perov...
- Autores:
-
Jaramillo Palacio, Johny Andrés
Barrera Bello, Elixir William
Munévar Cagigas, Julián Andrés
Arnache Olmos, Oscar Luis
Landínez Téllez, David A.
Roa Rojas, Jairo
- Tipo de recurso:
- Article of investigation
- Fecha de publicación:
- 2017
- Institución:
- Universidad de Antioquia
- Repositorio:
- Repositorio UdeA
- Idioma:
- eng
- OAI Identifier:
- oai:bibliotecadigital.udea.edu.co:10495/10968
- Acceso en línea:
- http://hdl.handle.net/10495/10968
- Palabra clave:
- Propiedades físicas
Physical Phenomena
Semiconductores
Semiconductors
Método Pechini modificado
Doble perovskita
Ferromagnético
http://aims.fao.org/aos/agrovoc/c_8e15773e
- Rights
- openAccess
- License
- Atribución-NoComercial-SinDerivadas 2.5 Colombia
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| dc.title.spa.fl_str_mv |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| title |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| spellingShingle |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method Propiedades físicas Physical Phenomena Semiconductores Semiconductors Método Pechini modificado Doble perovskita Ferromagnético http://aims.fao.org/aos/agrovoc/c_8e15773e |
| title_short |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| title_full |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| title_fullStr |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| title_full_unstemmed |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| title_sort |
Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method |
| dc.creator.fl_str_mv |
Jaramillo Palacio, Johny Andrés Barrera Bello, Elixir William Munévar Cagigas, Julián Andrés Arnache Olmos, Oscar Luis Landínez Téllez, David A. Roa Rojas, Jairo |
| dc.contributor.author.none.fl_str_mv |
Jaramillo Palacio, Johny Andrés Barrera Bello, Elixir William Munévar Cagigas, Julián Andrés Arnache Olmos, Oscar Luis Landínez Téllez, David A. Roa Rojas, Jairo |
| dc.subject.decs.none.fl_str_mv |
Propiedades físicas Physical Phenomena |
| topic |
Propiedades físicas Physical Phenomena Semiconductores Semiconductors Método Pechini modificado Doble perovskita Ferromagnético http://aims.fao.org/aos/agrovoc/c_8e15773e |
| dc.subject.agrovoc.none.fl_str_mv |
Semiconductores Semiconductors |
| dc.subject.proposal.spa.fl_str_mv |
Método Pechini modificado Doble perovskita Ferromagnético |
| dc.subject.agrovocuri.none.fl_str_mv |
http://aims.fao.org/aos/agrovoc/c_8e15773e |
| description |
ABSTRACT: In this paper the synthesis of the LaBiFe2O6 material by the modified Pechini method is reported. Structural, morphologic, magnetic and optic experimental studies were performed. Rietveld refinement of x-ray diffraction patterns revealed that LaBiFe2O6 crystallizes in an orthorhombic perovskite structure (space group Pnma, # 62). Scanning electron microscopy images showed the nanometric feature of grains. X-ray dispersive spectroscopy permitted to infer the obtaining of the LaBiFe2O6 expected stoichiometry. Results of magnetic susceptibility as a function of temperature and field magnetization evidenced mixed ferromagnetism and superparamagnetism behavior at T=300 K. Mössbauer spectroscopy supported the superparamagnetic and ferromagnetic responses as a result of the nanogranular morphology and anisotropy effects. Spectrum of diffuse reflectance suggest that this material behaves as a semiconductor with energy gap Eg=2.13 eV. |
| publishDate |
2017 |
| dc.date.issued.none.fl_str_mv |
2017 |
| dc.date.accessioned.none.fl_str_mv |
2019-05-02T19:37:44Z |
| dc.date.available.none.fl_str_mv |
2019-05-02T19:37:44Z |
| dc.type.spa.fl_str_mv |
info:eu-repo/semantics/article |
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http://purl.org/coar/version/c_970fb48d4fbd8a85 http://purl.org/coar/version/c_71e4c1898caa6e32 |
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http://purl.org/coar/resource_type/c_2df8fbb1 |
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https://purl.org/redcol/resource_type/ART |
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Artículo de investigación |
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http://purl.org/coar/resource_type/c_2df8fbb1 |
| dc.identifier.citation.spa.fl_str_mv |
Jaramillo, J. A., Barrera, E., Munévar, J. A., Arnache, O. L., Landínez, D. A., & Roa, J. (2017). Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method. Materials Research. 20(5), 1309-1316. DOI:10.1590/1980-5373-MR-2017-0290 |
| dc.identifier.issn.none.fl_str_mv |
1516-1439 |
| dc.identifier.uri.none.fl_str_mv |
http://hdl.handle.net/10495/10968 |
| dc.identifier.doi.none.fl_str_mv |
10.1590/1980-5373-MR-2017-0290 |
| dc.identifier.eissn.none.fl_str_mv |
1980-5373 |
| identifier_str_mv |
Jaramillo, J. A., Barrera, E., Munévar, J. A., Arnache, O. L., Landínez, D. A., & Roa, J. (2017). Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method. Materials Research. 20(5), 1309-1316. DOI:10.1590/1980-5373-MR-2017-0290 1516-1439 10.1590/1980-5373-MR-2017-0290 1980-5373 |
| url |
http://hdl.handle.net/10495/10968 |
| dc.language.iso.spa.fl_str_mv |
eng |
| language |
eng |
| dc.relation.ispartofjournalabbrev.spa.fl_str_mv |
Mat. Res. |
| dc.rights.*.fl_str_mv |
Atribución-NoComercial-SinDerivadas 2.5 Colombia |
| dc.rights.spa.fl_str_mv |
info:eu-repo/semantics/openAccess |
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http://creativecommons.org/licenses/by-nc-nd/2.5/co/ |
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https://creativecommons.org/licenses/by-nc-nd/4.0/ |
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Atribución-NoComercial-SinDerivadas 2.5 Colombia http://creativecommons.org/licenses/by-nc-nd/2.5/co/ http://purl.org/coar/access_right/c_abf2 https://creativecommons.org/licenses/by-nc-nd/4.0/ |
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openAccess |
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application/pdf |
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Universidade Federal de São Carlos (UFSCar) |
| dc.publisher.group.spa.fl_str_mv |
Grupo Estado Sólido |
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Brasil |
| institution |
Universidad de Antioquia |
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Jaramillo Palacio, Johny AndrésBarrera Bello, Elixir WilliamMunévar Cagigas, Julián AndrésArnache Olmos, Oscar LuisLandínez Téllez, David A.Roa Rojas, Jairo2019-05-02T19:37:44Z2019-05-02T19:37:44Z2017Jaramillo, J. A., Barrera, E., Munévar, J. A., Arnache, O. L., Landínez, D. A., & Roa, J. (2017). Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini Method. Materials Research. 20(5), 1309-1316. DOI:10.1590/1980-5373-MR-2017-02901516-1439http://hdl.handle.net/10495/1096810.1590/1980-5373-MR-2017-02901980-5373ABSTRACT: In this paper the synthesis of the LaBiFe2O6 material by the modified Pechini method is reported. Structural, morphologic, magnetic and optic experimental studies were performed. Rietveld refinement of x-ray diffraction patterns revealed that LaBiFe2O6 crystallizes in an orthorhombic perovskite structure (space group Pnma, # 62). Scanning electron microscopy images showed the nanometric feature of grains. X-ray dispersive spectroscopy permitted to infer the obtaining of the LaBiFe2O6 expected stoichiometry. Results of magnetic susceptibility as a function of temperature and field magnetization evidenced mixed ferromagnetism and superparamagnetism behavior at T=300 K. Mössbauer spectroscopy supported the superparamagnetic and ferromagnetic responses as a result of the nanogranular morphology and anisotropy effects. Spectrum of diffuse reflectance suggest that this material behaves as a semiconductor with energy gap Eg=2.13 eV.application/pdfengUniversidade Federal de São Carlos (UFSCar)Grupo Estado SólidoBrasilinfo:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_2df8fbb1https://purl.org/redcol/resource_type/ARTArtículo de investigaciónhttp://purl.org/coar/version/c_970fb48d4fbd8a85http://purl.org/coar/version/c_71e4c1898caa6e32Atribución-NoComercial-SinDerivadas 2.5 Colombiainfo:eu-repo/semantics/openAccesshttp://creativecommons.org/licenses/by-nc-nd/2.5/co/http://purl.org/coar/access_right/c_abf2https://creativecommons.org/licenses/by-nc-nd/4.0/Structure and physical properties of the LaBiFe2O6 Perovskite produced by the Modified Pechini MethodPropiedades físicasPhysical PhenomenaSemiconductoresSemiconductorsMétodo Pechini modificadoDoble perovskitaFerromagnéticohttp://aims.fao.org/aos/agrovoc/c_8e15773eMat. Res.Universidade Federal de São Carlos (UFSCar)13091316205ORIGINALArnacheOscar_2017_StructurePhysicalProperties.pdfArnacheOscar_2017_StructurePhysicalProperties.pdfArtículo de investigaciónapplication/pdf4741774https://bibliotecadigital.udea.edu.co/bitstream/10495/10968/1/ArnacheOscar_2017_StructurePhysicalProperties.pdfb4fa4b0c2e514f0c2d6765c10d593cf8MD51CC-LICENSElicense_urllicense_urltext/plain; charset=utf-849https://bibliotecadigital.udea.edu.co/bitstream/10495/10968/2/license_url4afdbb8c545fd630ea7db775da747b2fMD52license_textlicense_texttext/html; charset=utf-80https://bibliotecadigital.udea.edu.co/bitstream/10495/10968/3/license_textd41d8cd98f00b204e9800998ecf8427eMD53license_rdflicense_rdfLicenciaapplication/rdf+xml; charset=utf-80https://bibliotecadigital.udea.edu.co/bitstream/10495/10968/4/license_rdfd41d8cd98f00b204e9800998ecf8427eMD54LICENSElicense.txtlicense.txttext/plain; charset=utf-81748https://bibliotecadigital.udea.edu.co/bitstream/10495/10968/5/license.txt8a4605be74aa9ea9d79846c1fba20a33MD5510495/10968oai:bibliotecadigital.udea.edu.co:10495/109682023-09-26 11:49:35.435Repositorio Institucional Universidad de Antioquiaandres.perez@udea.edu.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 |