Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz

En el presente trabajo, fueron preparados materiales compuestos a partir de polipropileno reciclado (PPr) y celulosa de la cascarilla de arroz (Cel) empleando como agente de acoplamiento un polipropileno funcionalizado con un poliéster poliol altamente ramificado maleinizado (PP-g-MHBP). Por otra pa...

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Autores:
Contreras Atuesta, Ingrid Yuliani
Tipo de recurso:
Trabajo de grado de pregrado
Fecha de publicación:
2023
Institución:
Universidad Francisco de Paula Santander
Repositorio:
Repositorio Digital UFPS
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OAI Identifier:
oai:repositorio.ufps.edu.co:ufps/7721
Acceso en línea:
https://repositorio.ufps.edu.co/handle/ufps/7721
Palabra clave:
Polipropileno reciclado
Celulosa Cristalina
Materiales compuestos
Acoplamiento
Propiedades
Polipropileno reciclado
Materiales compuestos
Celulosa cristalina
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openAccess
License
Atribución-NoComercial-CompartirIgual 4.0 Internacional (CC BY-NC-SA 4.0)
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oai_identifier_str oai:repositorio.ufps.edu.co:ufps/7721
network_acronym_str RUFPS2
network_name_str Repositorio Digital UFPS
repository_id_str
dc.title.spa.fl_str_mv Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
title Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
spellingShingle Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
Polipropileno reciclado
Celulosa Cristalina
Materiales compuestos
Acoplamiento
Propiedades
Polipropileno reciclado
Materiales compuestos
Celulosa cristalina
title_short Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
title_full Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
title_fullStr Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
title_full_unstemmed Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
title_sort Evaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arroz
dc.creator.fl_str_mv Contreras Atuesta, Ingrid Yuliani
dc.contributor.advisor.none.fl_str_mv Murillo Ruiz, Edwin Alberto
dc.contributor.author.none.fl_str_mv Contreras Atuesta, Ingrid Yuliani
dc.contributor.jury.none.fl_str_mv Reyes Gómez, Sonia Esperanza
Parra Llanos, John Wilmer
dc.subject.lemb.spa.fl_str_mv Polipropileno reciclado
Celulosa Cristalina
Materiales compuestos
Acoplamiento
Propiedades
topic Polipropileno reciclado
Celulosa Cristalina
Materiales compuestos
Acoplamiento
Propiedades
Polipropileno reciclado
Materiales compuestos
Celulosa cristalina
dc.subject.proposal.spa.fl_str_mv Polipropileno reciclado
Materiales compuestos
Celulosa cristalina
description En el presente trabajo, fueron preparados materiales compuestos a partir de polipropileno reciclado (PPr) y celulosa de la cascarilla de arroz (Cel) empleando como agente de acoplamiento un polipropileno funcionalizado con un poliéster poliol altamente ramificado maleinizado (PP-g-MHBP). Por otra parte, para evaluar las propiedades estructurales, térmicas, reológicas, morfológicas y mecánicas de los materiales se realizaron los siguientes análisis: infrarrojo, difracción de rayos X, termogravimétrico, calorimetría de barrido diferencial, reológico, microscopia de barrido electrónico, absorción de humedad, absorción de agua y espesor de hinchamiento, índice de fluidez, dureza, resistencia al impacto, tracción y conductividad térmica. La Cel redujo la cristalinidad del PPr, pero el PP-g-MHBP no afectó apreciablemente las fases cristalinas del PPr y la Cel. La cristalinidad, la adhesión interfacial, la resistencia al impacto y la conductividad térmica de las mezclas, incrementaron con el contenido de PP-g-MHBP. Además, el PP-g-MHBP también mejoró la estabilidad térmica y actúo como agente plastificante, y acoplante para las mezclas de PPr/Cel. La mejor interacción entre el PPr y la Cel fue obtenida empleando un 20 % del PP-g-MHBP. Además, el módulo elástico, la fuerza tensil y la elongación a la ruptura no mostraron una dependencia con el contenido de PP-g-MHBP.
publishDate 2023
dc.date.issued.none.fl_str_mv 2023
dc.date.accessioned.none.fl_str_mv 2024-06-13T20:44:56Z
dc.date.available.none.fl_str_mv 2024-06-13T20:44:56Z
dc.type.none.fl_str_mv Trabajo de grado - Pregrado
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status_str acceptedVersion
dc.identifier.uri.none.fl_str_mv https://repositorio.ufps.edu.co/handle/ufps/7721
dc.identifier.instname.none.fl_str_mv instname:Universidad Francisco de Paula Santander
dc.identifier.reponame.none.fl_str_mv reponame:Repositorio Digital UFPS
dc.identifier.repourl.none.fl_str_mv repourl:https://repositorio.ufps.edu.co/
dc.identifier.signature.spa.fl_str_mv TQI V00002/2023
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identifier_str_mv instname:Universidad Francisco de Paula Santander
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TQI V00002/2023
dc.rights.spa.fl_str_mv Derechos Reservados - Universidad Francisco de Paula Santander, 2023
dc.rights.license.spa.fl_str_mv Atribución-NoComercial-CompartirIgual 4.0 Internacional (CC BY-NC-SA 4.0)
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rights_invalid_str_mv Atribución-NoComercial-CompartirIgual 4.0 Internacional (CC BY-NC-SA 4.0)
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https://creativecommons.org/licenses/by-nc-sa/4.0/
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dc.format.none.fl_str_mv application/pdf
dc.format.extent.none.fl_str_mv 157 páginas. ilustraciones, (Trabajo completo) 3.843 KB
dc.publisher.spa.fl_str_mv Universidad Francisco de Paula Santander
dc.publisher.faculty.spa.fl_str_mv Facultad de Ciencias Básicas
dc.publisher.place.spa.fl_str_mv San José de Cúcuta
dc.publisher.program.spa.fl_str_mv Química Industrial
dc.source.none.fl_str_mv https://catalogobiblioteca.ufps.edu.co/descargas/tesis/TG_1950020.pdf
institution Universidad Francisco de Paula Santander
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spelling Atribución-NoComercial-CompartirIgual 4.0 Internacional (CC BY-NC-SA 4.0)Derechos Reservados - Universidad Francisco de Paula Santander, 2023https://creativecommons.org/licenses/by-nc-sa/4.0/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Murillo Ruiz, Edwin Alberto632e87fd4ef6faae4ebcedb2ffed964eContreras Atuesta, Ingrid Yuliani33a67ab1c95407620ed1d6480689859dReyes Gómez, Sonia EsperanzaParra Llanos, John Wilmer2024-06-13T20:44:56Z2024-06-13T20:44:56Z2023https://repositorio.ufps.edu.co/handle/ufps/7721instname:Universidad Francisco de Paula Santanderreponame:Repositorio Digital UFPSrepourl:https://repositorio.ufps.edu.co/TQI V00002/2023En el presente trabajo, fueron preparados materiales compuestos a partir de polipropileno reciclado (PPr) y celulosa de la cascarilla de arroz (Cel) empleando como agente de acoplamiento un polipropileno funcionalizado con un poliéster poliol altamente ramificado maleinizado (PP-g-MHBP). Por otra parte, para evaluar las propiedades estructurales, térmicas, reológicas, morfológicas y mecánicas de los materiales se realizaron los siguientes análisis: infrarrojo, difracción de rayos X, termogravimétrico, calorimetría de barrido diferencial, reológico, microscopia de barrido electrónico, absorción de humedad, absorción de agua y espesor de hinchamiento, índice de fluidez, dureza, resistencia al impacto, tracción y conductividad térmica. La Cel redujo la cristalinidad del PPr, pero el PP-g-MHBP no afectó apreciablemente las fases cristalinas del PPr y la Cel. La cristalinidad, la adhesión interfacial, la resistencia al impacto y la conductividad térmica de las mezclas, incrementaron con el contenido de PP-g-MHBP. Además, el PP-g-MHBP también mejoró la estabilidad térmica y actúo como agente plastificante, y acoplante para las mezclas de PPr/Cel. La mejor interacción entre el PPr y la Cel fue obtenida empleando un 20 % del PP-g-MHBP. Además, el módulo elástico, la fuerza tensil y la elongación a la ruptura no mostraron una dependencia con el contenido de PP-g-MHBP.1. INTRODUCCIÓN 1 2. PLANTEAMIENTO DEL PROBLEMA 3 3. JUSTIFICACIÓN 8 4. MARCO REFERENCIAL 12 4.1. ESTADO DEL ARTE 12 4.2. MARCO TEÓRICO 16 4.2.1. PP 16 4.2.2. Funcionalización de las poliolefinas 18 4.2.3. Fibras naturales 20 4.2.4. CA 21 4.2.5. Materiales compuestos de fibras naturales 22 4.2.6. Economía circular 24 4.2.7. Análisis de ciclo de vida (LCA) 27 4.2.8. ANOVA 27 4.3. MARCO CONCEPTUAL 30 4.3.1. Agentes de acoplamiento. 30 4.3.2. Análisis multivariante. 30 4.3.3. Compatibilización. 30 4.3.4. Cradle to Cradle (C2C). 30 4.3.5. Cradle to Grave. 30 4.3.6. Distribución normal. 31 4.3.7. Elongación a la ruptura. 31 4.3.8. Fuerza ténsil. 31 4.3.9. Funcionalización. 31 4.3.10. Hipótesis nula (H0). 32 4.3.11. Hipótesis alternativa (Ha o H1). 32 4.3.12. Hipótesis operacional. 32 4.3.13. Hipótesis estadística. 32 4.3.14. Intersección. 32 4.3.15. Material compuesto. 33 4.3.16. Medias marginales 33 4.3.17. Modelo ANOVA de efectos fijos 33 4.3.18. Modelo ANOVA de efectos aleatorios 33 4.3.19. Modelo corregido 33 4.3.20. Modulo ténsil o tracción 34 4.3.21. Objetivos de desarrollo sostenible 34 4.3.22. Prueba de los efectos inter-sujetos 34 4.3.23. Prueba F 34 4.3.24. Reciclar 35 4.3.25. Relleno 35 4.3.26. Reducir 35 4.3.27. Reutilizar 35 4.3.28. Variable 36 4.3.29. Variable dependiente 36 4.3.30. Variable independiente 36 4.3.31. Variable métrica o cuantitativas 36 4.3.32. Variable no métrica o cualitativas 36 4.3.33. Varianza de error 37 4.4. MARCO LEGAL 37 4.4.1. Legislación internacional 37 4.4.1.1. Convenios internacionales 37 4.4.2. Legislación nacional 39 5. OBJETIVOS 40 5.1. Objetivo General 40 5.2. Objetivos específicos 40 6. METODOLOGÍA 41 6.1. DISEÑO EXPERIMENTAL 41 6.2. PROCEDIMIENTO EXPERIMENTAL 41 6.2.1. Materiales 41 6.2.2. Preparación de los materiales 42 6.2.3. Caracterización de los materiales 45 7. ANALISIS Y DISCUSIÓN DE LOS RESULTADOS 49 7.1. Obtención de la Cel 49 7.2. Análisis granulométrico 49 7.2. Reometría de torque 50 7.3. Análisis IR 52 7.4. DRX 54 7.5. TGA 56 7.6. DSC 60 7.7. Reología 63 7.7.1. Análisis estático 63 7.7.1. Energía de activación 65 7.7.2. Amplitud sweep 68 7.7.3. Análisis oscilatorio 69 7.7.4. Comportamiento de G' y G'' 70 7.7.5. Regla de Cox-Merz 72 7.7.6. Tiempos de relajación 74 7.7.7. Diagrama de Van Gurp-Palmen 75 7.7.8. Diagrama de Cole-Cole 76 7.8. SEM 78 7.9. AH 80 7.10. AbA y el EH 82 7.11. MFI 84 7.12. Dureza 85 7.13. Resistencia al impacto 86 7.14. Tracción 87 7.15. Conductividad térmica 89 7.16. Resultados ANOVA 91 7.16.1. Hipótesis Operacional 91 7.16.2. Hipótesis Estadística 91 7.16.3. Análisis de Resultados 91 7.17. PROTOTIPO 103 8. CONCLUSIONES 107 9. PERSPECTIVAS DEL TRABAJO 108 10. PRODUCCIÓN CIENTÍFICA 109 11. REFERENCIAS 112Archivo Medios ElectrónicosPregradoQuímico Industrialapplication/pdf157 páginas. ilustraciones, (Trabajo completo) 3.843 KBUniversidad Francisco de Paula SantanderFacultad de Ciencias BásicasSan José de CúcutaQuímica Industrialhttps://catalogobiblioteca.ufps.edu.co/descargas/tesis/TG_1950020.pdfEvaluación de un polipropileno funcionalizado con un poliéster altamente ramificado maleinizado, como agente de acoplamiento para materiales compuestos de polipropileno reciclado y celulosa de la cascarilla de arrozTrabajo de grado - Pregradohttp://purl.org/coar/resource_type/c_7a1fTextinfo:eu-repo/semantics/bachelorThesishttp://purl.org/redcol/resource_type/TPinfo:eu-repo/semantics/acceptedVersionPolipropileno recicladoCelulosa CristalinaMateriales compuestosAcoplamientoPropiedadesPolipropileno recicladoMateriales compuestosCelulosa cristalinaAcharya, S., & Chaudhary, A. (2012). Bioprospecting thermophiles for cellulase production: A review. Brazilian Journal of Microbiology, 43(3), 844–856. https://doi.org/10.1590/S151783822012000300001Ahmad, Z., Roziaizan, N. N., Rahman, R., Mohamad, A. F., & Wan Ismail, W. I. N. (2016). Isolation and characterization of Microcrystalline Cellulose (MCC) from Rice Husk (RH). MATEC Web of Conferences, 47(January). https://doi.org/10.1051/matecconf/20164705013Alqahtani, N., Alejji, M., & Labidi, S. (2021). Influence of Compatibilizers on Date Palm Fiber and High Density Polyethylene Composite. American Journal of Engineering, Science and Technology (AJEST), 10(MARCH 2021), 62–81.Ararat, C. A., Quiñonez, W., & Murillo, E. A. (2019). Maleinized Hyperbranched Polyol Polyester: Effect of the Content of Maleic Anhydride in the Structural, Thermal and Rheological Properties. Macromolecular Research, 27(7), 693–702. https://doi.org/10.1007/s13233-0197089-1Ariyoshi, S., Hashimoto, S., Ohnishi, S., Negishi, S., Mikami, H., Hayashi, K., Tanaka, S., & Hiroshiba, N. (2021). 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A kind of nano-cellulose reinforced polypropylene foamed material and preparation method thereof.ORIGINALTG_1950020.pdfTG_1950020.pdfProyecto de Pregradoapplication/pdf3934650https://repositorio.ufps.edu.co/bitstream/ufps/7721/1/TG_1950020.pdffb869c286d475bff28525059b12848d7MD51open accessTEXTTG_1950020.pdf.txtTG_1950020.pdf.txtExtracted texttext/plain250021https://repositorio.ufps.edu.co/bitstream/ufps/7721/2/TG_1950020.pdf.txtd40bcc4cb5f926157c6fe135bc09defeMD52open accessTHUMBNAILTG_1950020.pdf.jpgTG_1950020.pdf.jpgGenerated Thumbnailimage/jpeg16446https://repositorio.ufps.edu.co/bitstream/ufps/7721/3/TG_1950020.pdf.jpgeb6f924220b439935693800d57716838MD53open accessufps/7721oai:repositorio.ufps.edu.co:ufps/77212024-09-24 03:01:15.711An error occurred on the license name.|||https://creativecommons.org/licenses/by-nc-sa/4.0/open accessRepositorio Universidad Francisco de Paula Santanderbdigital@metabiblioteca.com

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