Vibrational Raman modes and particle size analysis of cupric oxide with calcination temperature
In this work a study of the effect of the synthesis conditions on the vibratory and particle size properties in the cupric oxide (CuO) has been presented. The synthesis has been carried out by the polymeric precursor method without modifying the PH in the process, this being a low cost method. The s...
- Autores:
-
Raba, Angela
Rincón Joya, Miryam
Barba, Jose
- Tipo de recurso:
- Article of journal
- Fecha de publicación:
- 2019
- Institución:
- Universidad Francisco de Paula Santander
- Repositorio:
- Repositorio Digital UFPS
- Idioma:
- eng
- OAI Identifier:
- oai:repositorio.ufps.edu.co:ufps/2723
- Acceso en línea:
- http://repositorio.ufps.edu.co/handle/ufps/2723
- Palabra clave:
- Synthesis
Cupric
Particle
Spectroscopy
- Rights
- openAccess
- License
- http://purl.org/coar/access_right/c_abf2
| Summary: | In this work a study of the effect of the synthesis conditions on the vibratory and particle size properties in the cupric oxide (CuO) has been presented. The synthesis has been carried out by the polymeric precursor method without modifying the PH in the process, this being a low cost method. The samples obtained have been subjected to several calcination temperatures, 450 °C, 550 °C, 650 °C and 800 °C. In particle analysis by X-ray, scanning electron microscopy (SEM) and statistical it has been observed that for very low or very high calcination temperatures the particle size increases, finding 650 °C as the best calcination temperature. In the Raman spectra, the Ag and Bg vibration have been presented in the samples, with the peaks being narrower for the temperature of 450 °C. |
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