Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil

The biodiesel is obtained from about 10 years ago in Europe, and now that it has taken hold as fuel for diesel engines, it is expected a clear increase in the production of this class of fuels in a the near future. The biodiesel is derived from the transesterification reaction of castor oil with met...

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Tipo de recurso:
http://purl.org/coar/resource_type/c_6622
Fecha de publicación:
2012
Institución:
Universidad Pedagógica y Tecnológica de Colombia
Repositorio:
RiUPTC: Repositorio Institucional UPTC
Idioma:
spa
OAI Identifier:
oai:repositorio.uptc.edu.co:001/12194
Acceso en línea:
https://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380
https://repositorio.uptc.edu.co/handle/001/12194
Palabra clave:
glycerol
obtaining
purification
separation
characterization
castor oil
glicerol
obtención
separación
purificación
caracterización
aceite de higuerilla
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License
Derechos de autor 2012 Ingeniería Investigación y Desarrollo
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oai_identifier_str oai:repositorio.uptc.edu.co:001/12194
network_acronym_str REPOUPTC2
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dc.title.en-US.fl_str_mv Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
dc.title.es-ES.fl_str_mv Proceso integral de obtención de glicerol como subproducto de la producción de biodiésel, a partir del aceite de higuerilla
title Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
spellingShingle Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
glycerol
obtaining
purification
separation
characterization
castor oil
glicerol
obtención
separación
purificación
caracterización
aceite de higuerilla
title_short Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
title_full Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
title_fullStr Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
title_full_unstemmed Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
title_sort Integral process of obtaining glycerol as a by-product of biodiesel production from castor oil
dc.subject.en-US.fl_str_mv glycerol
obtaining
purification
separation
characterization
castor oil
topic glycerol
obtaining
purification
separation
characterization
castor oil
glicerol
obtención
separación
purificación
caracterización
aceite de higuerilla
dc.subject.es-ES.fl_str_mv glicerol
obtención
separación
purificación
caracterización
aceite de higuerilla
description The biodiesel is obtained from about 10 years ago in Europe, and now that it has taken hold as fuel for diesel engines, it is expected a clear increase in the production of this class of fuels in a the near future. The biodiesel is derived from the transesterification reaction of castor oil with methanol, which is the main by-product the glycerol with an approximate content of 10%. Besides catalyst residuals, soaps, methanol traces, mono and diglycerides in small percentages are presented. This study proposes the separation, purification and characterization of the glycerol obtained from the transesterificación reaction of the castor oil, in order to be able to market it in the national or international market, so that it fulfills the standards of quality, which means getting a pure glycerol and the appropriate physico-chemical characteristics and techniques. The glycerin-methyl esters separation is carried out by decantation being obtained a percentage of around 70% glycerol. This percentage is subsequently increased through the purification process, using hydrochloric acid. Glycerol characterization was carried out by physicochemical and organoleptic tests. The purification process allowed us to obtain a glycerol with a percentage of purity close to 98%. It was also tested by comparison with theoretical data that remnants influenced in the physiochemical properties
publishDate 2012
dc.date.accessioned.none.fl_str_mv 2024-07-05T18:47:42Z
dc.date.available.none.fl_str_mv 2024-07-05T18:47:42Z
dc.date.none.fl_str_mv 2012-12-01
dc.type.none.fl_str_mv info:eu-repo/semantics/article
dc.type.coar.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
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dc.type.coar.spa.fl_str_mv http://purl.org/coar/resource_type/c_6622
dc.type.coarversion.spa.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a206
format http://purl.org/coar/resource_type/c_6622
dc.identifier.none.fl_str_mv https://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380
dc.identifier.uri.none.fl_str_mv https://repositorio.uptc.edu.co/handle/001/12194
url https://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380
https://repositorio.uptc.edu.co/handle/001/12194
dc.language.none.fl_str_mv spa
dc.language.iso.none.fl_str_mv spa
language spa
dc.relation.none.fl_str_mv https://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380/3013
dc.rights.es-ES.fl_str_mv Derechos de autor 2012 Ingeniería Investigación y Desarrollo
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.rights.coar.spa.fl_str_mv http://purl.org/coar/access_right/c_abf123
rights_invalid_str_mv Derechos de autor 2012 Ingeniería Investigación y Desarrollo
http://purl.org/coar/access_right/c_abf123
http://purl.org/coar/access_right/c_abf2
dc.format.none.fl_str_mv application/pdf
dc.publisher.es-ES.fl_str_mv Universidad Pedagógica y Tecnológica de Colombia - UPTC
dc.source.en-US.fl_str_mv Ingeniería Investigación y Desarrollo; Vol. 12 No. 2: julio-diciembre de 2012; 9-14
dc.source.es-ES.fl_str_mv Ingeniería Investigación y Desarrollo; Vol. 12 Núm. 2: julio-diciembre de 2012; 9-14
dc.source.none.fl_str_mv 2422-4324
1900-771X
institution Universidad Pedagógica y Tecnológica de Colombia
repository.name.fl_str_mv Repositorio Institucional UPTC
repository.mail.fl_str_mv repositorio.uptc@uptc.edu.co
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spelling 2012-12-012024-07-05T18:47:42Z2024-07-05T18:47:42Zhttps://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380https://repositorio.uptc.edu.co/handle/001/12194The biodiesel is obtained from about 10 years ago in Europe, and now that it has taken hold as fuel for diesel engines, it is expected a clear increase in the production of this class of fuels in a the near future. The biodiesel is derived from the transesterification reaction of castor oil with methanol, which is the main by-product the glycerol with an approximate content of 10%. Besides catalyst residuals, soaps, methanol traces, mono and diglycerides in small percentages are presented. This study proposes the separation, purification and characterization of the glycerol obtained from the transesterificación reaction of the castor oil, in order to be able to market it in the national or international market, so that it fulfills the standards of quality, which means getting a pure glycerol and the appropriate physico-chemical characteristics and techniques. The glycerin-methyl esters separation is carried out by decantation being obtained a percentage of around 70% glycerol. This percentage is subsequently increased through the purification process, using hydrochloric acid. Glycerol characterization was carried out by physicochemical and organoleptic tests. The purification process allowed us to obtain a glycerol with a percentage of purity close to 98%. It was also tested by comparison with theoretical data that remnants influenced in the physiochemical propertiesEl biodiésel es obtenido desde hace cerca de diez años en Europa, pero ahora, que ha tomado fuerza como combustible para motores diésel, se espera un claro aumento en la producción de esta clase de combustibles en un futuro próximo. El biodiésel es obtenido de la reacción de transesterificación de aceite de higuerilla con metanol, de la cual resulta como subproducto principal el glicerol, con un contenido aproximado del 10 %. Además se presentan residuos de catalizador, jabones, restos de metanol, mono y diglicéridos en pequeños porcentajes. En este estudio se plantea la separación, purificación y caracterización del glicerol obtenido a partir de la reacción de transesterificación del aceite de higuerilla, con el propósito de poder comercializarlo en el mercado nacional o internacional, de manera que cumpla con los estándares de calidad, lo cual significa obtener un glicerol puro y con las características fisicoquímicas y técnicas adecuadas. La separación glicerina–esteres metílicos se realiza por decantación, obteniéndose un porcentaje de glicerol cercano al 70 %. Este porcentaje es aumentado posteriormente mediante el proceso de purificación, utilizando ácido clorhídrico. La caracterización del glicerol fue llevada a cabo mediante pruebas fisicoquímicas y organolépticas. El proceso de purificación permitió obtener un glicerol con un porcentaje de pureza cercano al 98 %. También se comprobó, por la comparación con datos teóricos, que los remanentes influyeron en las propiedades fisicoquímicas.application/pdfspaspaUniversidad Pedagógica y Tecnológica de Colombia - UPTChttps://revistas.uptc.edu.co/index.php/ingenieria_sogamoso/article/view/3380/3013Derechos de autor 2012 Ingeniería Investigación y Desarrollohttp://purl.org/coar/access_right/c_abf123http://purl.org/coar/access_right/c_abf2Ingeniería Investigación y Desarrollo; Vol. 12 No. 2: julio-diciembre de 2012; 9-14Ingeniería Investigación y Desarrollo; Vol. 12 Núm. 2: julio-diciembre de 2012; 9-142422-43241900-771Xglycerolobtainingpurificationseparationcharacterizationcastor oilglicerolobtenciónseparaciónpurificacióncaracterizaciónaceite de higuerillaIntegral process of obtaining glycerol as a by-product of biodiesel production from castor oilProceso integral de obtención de glicerol como subproducto de la producción de biodiésel, a partir del aceite de higuerillainfo:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6622http://purl.org/coar/resource_type/c_2df8fbb1http://purl.org/coar/version/c_970fb48d4fbd8a206http://purl.org/coar/version/c_970fb48d4fbd8a85Romero, LeonelCortez, RicardoSanchéz, LizzmaryPiracoca, MarcelaAyala, LinaBecerra-Castro, Yeimy001/12194oai:repositorio.uptc.edu.co:001/121942025-07-18 11:25:46.225metadata.onlyhttps://repositorio.uptc.edu.coRepositorio Institucional UPTCrepositorio.uptc@uptc.edu.co