Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TG...
- Autores:
-
Aparicio Rojas, Gladis Miriam
Florez Larrahondo, Tulio Andrés
Aparicio Rojas, Gladis Miriam
- Tipo de recurso:
- Article of journal
- Fecha de publicación:
- 2014
- Institución:
- Universidad Autónoma de Occidente
- Repositorio:
- RED: Repositorio Educativo Digital UAO
- Idioma:
- eng
- OAI Identifier:
- oai:red.uao.edu.co:10614/11580
- Acceso en línea:
- http://hdl.handle.net/10614/11580
- Palabra clave:
- Compost
Thermal analysis
Thermogravimetry (TGA)
Differential scanning calorimetry (DSC)
Mass spectrometry (MS)
Activation energy
Decomposition kinetics
Humus
- Rights
- openAccess
- License
- Derechos Reservados - Universidad Autónoma de Occidente
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dc.title.eng.fl_str_mv |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
title |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
spellingShingle |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt Compost Thermal analysis Thermogravimetry (TGA) Differential scanning calorimetry (DSC) Mass spectrometry (MS) Activation energy Decomposition kinetics Humus |
title_short |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
title_full |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
title_fullStr |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
title_full_unstemmed |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
title_sort |
Thermal Characterization and Lifetime Estimation of the Humus Lombricospt |
dc.creator.fl_str_mv |
Aparicio Rojas, Gladis Miriam Florez Larrahondo, Tulio Andrés Aparicio Rojas, Gladis Miriam |
dc.contributor.author.none.fl_str_mv |
Aparicio Rojas, Gladis Miriam Florez Larrahondo, Tulio Andrés Aparicio Rojas, Gladis Miriam |
dc.subject.armarc.spa.fl_str_mv |
Compost |
topic |
Compost Thermal analysis Thermogravimetry (TGA) Differential scanning calorimetry (DSC) Mass spectrometry (MS) Activation energy Decomposition kinetics Humus |
dc.subject.proposal.eng.fl_str_mv |
Thermal analysis Thermogravimetry (TGA) Differential scanning calorimetry (DSC) Mass spectrometry (MS) Activation energy Decomposition kinetics Humus |
description |
Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TGA) to study the equilibrium of phasesand Mass Spectrometry (MS) coupled to TGA to identify detached elements in a temperature range. The temperature range used in this study was 30˚C < T < 600˚C. The energy required for the water desorption in the humus has been found in this study. The humus showed a quick desorption between 30˚C ≤ TDesorption ≤ 110˚C at a heating rate of 10˚C/min and presented decomposition around 250˚C. Moreover, the kinetics of the desorption of the humus was studied to obtain the activation energy three TGA measures for three different heating rates. The average activation energy was about 26 kJ/Mol. This result was carried out to obtain an estimation of the desorption time of water in the range from room temperature to the decomposition temperature around 350˚C |
publishDate |
2014 |
dc.date.issued.none.fl_str_mv |
2014-01 |
dc.date.accessioned.none.fl_str_mv |
2019-11-26T20:25:32Z |
dc.date.available.none.fl_str_mv |
2019-11-26T20:25:32Z |
dc.type.spa.fl_str_mv |
Artículo de revista |
dc.type.coar.fl_str_mv |
http://purl.org/coar/resource_type/c_2df8fbb1 |
dc.type.coarversion.fl_str_mv |
http://purl.org/coar/version/c_970fb48d4fbd8a85 |
dc.type.coar.eng.fl_str_mv |
http://purl.org/coar/resource_type/c_6501 |
dc.type.content.eng.fl_str_mv |
Text |
dc.type.driver.eng.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.redcol.eng.fl_str_mv |
http://purl.org/redcol/resource_type/ARTREF |
dc.type.version.eng.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
http://purl.org/coar/resource_type/c_6501 |
status_str |
publishedVersion |
dc.identifier.citation.eng.fl_str_mv |
Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.52007 |
dc.identifier.issn.spa.fl_str_mv |
21568251 (impreso) 21568278 (en línea) |
dc.identifier.uri.none.fl_str_mv |
http://hdl.handle.net/10614/11580 |
dc.identifier.doi.spa.fl_str_mv |
10.4236/ajac.2014.52007 |
identifier_str_mv |
Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.52007 21568251 (impreso) 21568278 (en línea) 10.4236/ajac.2014.52007 |
url |
http://hdl.handle.net/10614/11580 |
dc.language.iso.eng.fl_str_mv |
eng |
language |
eng |
dc.relation.citationendpage.none.fl_str_mv |
49 |
dc.relation.citationissue.none.fl_str_mv |
2 |
dc.relation.citationstartpage.none.fl_str_mv |
45 |
dc.relation.citationvolume.none.fl_str_mv |
5 |
dc.relation.ispartofjournal.eng.fl_str_mv |
American Journal of Analytical Chemistry |
dc.relation.references.none.fl_str_mv |
[1] G. W. H. Hö hne, W. F. Hemminger and H.-J. Flammersheim, “Differential Scanning Calorimetry,” 2nd Edition, Springer, Heidelberg, 2010, pp. 71-91. [2] F. J. Stevenson, “Humus Chemistry: Genesis, Composition, Reactions,” 2nd Edition, Wiley, 1994, pp. 188-208. [3] J. H. Flynn and L. A. Wall, “A Quick, Direct Method for the Determination of Activation Energy from Thermogravimetric Data,” Polymer Letters Vol. 4, No. 5, 1966, pp. 323-328. http://dx.doi.org/10.1002/pol.1966.110040504 [4] ASTM Test Method E1641, “Standard Test Method for Decomposition Kinetics by Thermogravimetry,” ASTM Book of Standards 14.02, American Society for Testing and Materials, 1994, pp. 1042-1046. [5] D. J. Toop, “Theory of Life Testing and Use of Thermogravimetric Analysis to Predict the Thermal Life of Wire Enamels,” IEEE Transactions on Electrical Insulation, Vol. EI-6, No. 1, 1971, pp. 2-14. |
dc.rights.spa.fl_str_mv |
Derechos Reservados - Universidad Autónoma de Occidente |
dc.rights.coar.fl_str_mv |
http://purl.org/coar/access_right/c_abf2 |
dc.rights.uri.eng.fl_str_mv |
https://creativecommons.org/licenses/by-nc-nd/4.0/ |
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info:eu-repo/semantics/openAccess |
dc.rights.creativecommons.spa.fl_str_mv |
Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0) |
rights_invalid_str_mv |
Derechos Reservados - Universidad Autónoma de Occidente https://creativecommons.org/licenses/by-nc-nd/4.0/ Atribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0) http://purl.org/coar/access_right/c_abf2 |
eu_rights_str_mv |
openAccess |
dc.format.eng.fl_str_mv |
application/pdf |
dc.format.extent.spa.fl_str_mv |
5 páginas |
dc.coverage.spatial.none.fl_str_mv |
Universidad Autónoma de Occidente. Calle 25 115-85. Km 2 vía Cali-Jamundí |
dc.publisher.eng.fl_str_mv |
Scientific Research |
institution |
Universidad Autónoma de Occidente |
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Aparicio Rojas, Gladis Miriamd68d65b992d8979830280e7b74533845Florez Larrahondo, Tulio Andrés80d7e0c71964763d6d1a0a797677eb55Aparicio Rojas, Gladis Miriamvirtual::304-1Universidad Autónoma de Occidente. Calle 25 115-85. Km 2 vía Cali-Jamundí2019-11-26T20:25:32Z2019-11-26T20:25:32Z2014-01Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.5200721568251 (impreso)21568278 (en línea)http://hdl.handle.net/10614/1158010.4236/ajac.2014.52007Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TGA) to study the equilibrium of phasesand Mass Spectrometry (MS) coupled to TGA to identify detached elements in a temperature range. The temperature range used in this study was 30˚C < T < 600˚C. The energy required for the water desorption in the humus has been found in this study. The humus showed a quick desorption between 30˚C ≤ TDesorption ≤ 110˚C at a heating rate of 10˚C/min and presented decomposition around 250˚C. Moreover, the kinetics of the desorption of the humus was studied to obtain the activation energy three TGA measures for three different heating rates. The average activation energy was about 26 kJ/Mol. 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W. H. Hö hne, W. F. Hemminger and H.-J. Flammersheim, “Differential Scanning Calorimetry,” 2nd Edition, Springer, Heidelberg, 2010, pp. 71-91.[2] F. J. Stevenson, “Humus Chemistry: Genesis, Composition, Reactions,” 2nd Edition, Wiley, 1994, pp. 188-208.[3] J. H. Flynn and L. A. Wall, “A Quick, Direct Method for the Determination of Activation Energy from Thermogravimetric Data,” Polymer Letters Vol. 4, No. 5, 1966, pp. 323-328. http://dx.doi.org/10.1002/pol.1966.110040504[4] ASTM Test Method E1641, “Standard Test Method for Decomposition Kinetics by Thermogravimetry,” ASTM Book of Standards 14.02, American Society for Testing and Materials, 1994, pp. 1042-1046.[5] D. J. 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