Thermal Characterization and Lifetime Estimation of the Humus Lombricospt

Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TG...

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Autores:
Aparicio Rojas, Gladis Miriam
Florez Larrahondo, Tulio Andrés
Aparicio Rojas, Gladis Miriam
Tipo de recurso:
Article of journal
Fecha de publicación:
2014
Institución:
Universidad Autónoma de Occidente
Repositorio:
RED: Repositorio Educativo Digital UAO
Idioma:
eng
OAI Identifier:
oai:red.uao.edu.co:10614/11580
Acceso en línea:
http://hdl.handle.net/10614/11580
Palabra clave:
Compost
Thermal analysis
Thermogravimetry (TGA)
Differential scanning calorimetry (DSC)
Mass spectrometry (MS)
Activation energy
Decomposition kinetics
Humus
Rights
openAccess
License
Derechos Reservados - Universidad Autónoma de Occidente
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dc.title.eng.fl_str_mv Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
title Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
spellingShingle Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
Compost
Thermal analysis
Thermogravimetry (TGA)
Differential scanning calorimetry (DSC)
Mass spectrometry (MS)
Activation energy
Decomposition kinetics
Humus
title_short Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
title_full Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
title_fullStr Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
title_full_unstemmed Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
title_sort Thermal Characterization and Lifetime Estimation of the Humus Lombricospt
dc.creator.fl_str_mv Aparicio Rojas, Gladis Miriam
Florez Larrahondo, Tulio Andrés
Aparicio Rojas, Gladis Miriam
dc.contributor.author.none.fl_str_mv Aparicio Rojas, Gladis Miriam
Florez Larrahondo, Tulio Andrés
Aparicio Rojas, Gladis Miriam
dc.subject.armarc.spa.fl_str_mv Compost
topic Compost
Thermal analysis
Thermogravimetry (TGA)
Differential scanning calorimetry (DSC)
Mass spectrometry (MS)
Activation energy
Decomposition kinetics
Humus
dc.subject.proposal.eng.fl_str_mv Thermal analysis
Thermogravimetry (TGA)
Differential scanning calorimetry (DSC)
Mass spectrometry (MS)
Activation energy
Decomposition kinetics
Humus
description Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TGA) to study the equilibrium of phasesand Mass Spectrometry (MS) coupled to TGA to identify detached elements in a temperature range. The temperature range used in this study was 30˚C < T < 600˚C. The energy required for the water desorption in the humus has been found in this study. The humus showed a quick desorption between 30˚C ≤ TDesorption ≤ 110˚C at a heating rate of 10˚C/min and presented decomposition around 250˚C. Moreover, the kinetics of the desorption of the humus was studied to obtain the activation energy three TGA measures for three different heating rates. The average activation energy was about 26 kJ/Mol. This result was carried out to obtain an estimation of the desorption time of water in the range from room temperature to the decomposition temperature around 350˚C
publishDate 2014
dc.date.issued.none.fl_str_mv 2014-01
dc.date.accessioned.none.fl_str_mv 2019-11-26T20:25:32Z
dc.date.available.none.fl_str_mv 2019-11-26T20:25:32Z
dc.type.spa.fl_str_mv Artículo de revista
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dc.type.content.eng.fl_str_mv Text
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dc.identifier.citation.eng.fl_str_mv Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.52007
dc.identifier.issn.spa.fl_str_mv 21568251 (impreso)
21568278 (en línea)
dc.identifier.uri.none.fl_str_mv http://hdl.handle.net/10614/11580
dc.identifier.doi.spa.fl_str_mv 10.4236/ajac.2014.52007
identifier_str_mv Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.52007
21568251 (impreso)
21568278 (en línea)
10.4236/ajac.2014.52007
url http://hdl.handle.net/10614/11580
dc.language.iso.eng.fl_str_mv eng
language eng
dc.relation.citationendpage.none.fl_str_mv 49
dc.relation.citationissue.none.fl_str_mv 2
dc.relation.citationstartpage.none.fl_str_mv 45
dc.relation.citationvolume.none.fl_str_mv 5
dc.relation.ispartofjournal.eng.fl_str_mv American Journal of Analytical Chemistry
dc.relation.references.none.fl_str_mv [1] G. W. H. Hö hne, W. F. Hemminger and H.-J. Flammersheim, “Differential Scanning Calorimetry,” 2nd Edition, Springer, Heidelberg, 2010, pp. 71-91.
[2] F. J. Stevenson, “Humus Chemistry: Genesis, Composition, Reactions,” 2nd Edition, Wiley, 1994, pp. 188-208.
[3] J. H. Flynn and L. A. Wall, “A Quick, Direct Method for the Determination of Activation Energy from Thermogravimetric Data,” Polymer Letters Vol. 4, No. 5, 1966, pp. 323-328. http://dx.doi.org/10.1002/pol.1966.110040504
[4] ASTM Test Method E1641, “Standard Test Method for Decomposition Kinetics by Thermogravimetry,” ASTM Book of Standards 14.02, American Society for Testing and Materials, 1994, pp. 1042-1046.
[5] D. J. Toop, “Theory of Life Testing and Use of Thermogravimetric Analysis to Predict the Thermal Life of Wire Enamels,” IEEE Transactions on Electrical Insulation, Vol. EI-6, No. 1, 1971, pp. 2-14.
dc.rights.spa.fl_str_mv Derechos Reservados - Universidad Autónoma de Occidente
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rights_invalid_str_mv Derechos Reservados - Universidad Autónoma de Occidente
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dc.publisher.eng.fl_str_mv Scientific Research
institution Universidad Autónoma de Occidente
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spelling Aparicio Rojas, Gladis Miriamd68d65b992d8979830280e7b74533845Florez Larrahondo, Tulio Andrés80d7e0c71964763d6d1a0a797677eb55Aparicio Rojas, Gladis Miriamvirtual::304-1Universidad Autónoma de Occidente. Calle 25 115-85. Km 2 vía Cali-Jamundí2019-11-26T20:25:32Z2019-11-26T20:25:32Z2014-01Aparicio Rojas, G. M ; Florez Larrahondo, T. A. Thermal Characterization and Lifetime Estimation of the Humus Lombricospt. American Journal of Analytical Chemistry. 5(2), (enero 2014); 45-49. DOI: 10.4236/ajac.2014.5200721568251 (impreso)21568278 (en línea)http://hdl.handle.net/10614/1158010.4236/ajac.2014.52007Through this study, the humus produced in the breeding place of Universidad Autonoma de Occidente was thermally characterized. The humus was submitted to a heating program controlled by the Differential Scanning Calorimetry (DSC) technique to characterize the type of transition, Thermogravimetry (TGA) to study the equilibrium of phasesand Mass Spectrometry (MS) coupled to TGA to identify detached elements in a temperature range. The temperature range used in this study was 30˚C < T < 600˚C. The energy required for the water desorption in the humus has been found in this study. The humus showed a quick desorption between 30˚C ≤ TDesorption ≤ 110˚C at a heating rate of 10˚C/min and presented decomposition around 250˚C. Moreover, the kinetics of the desorption of the humus was studied to obtain the activation energy three TGA measures for three different heating rates. The average activation energy was about 26 kJ/Mol. 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W. H. Hö hne, W. F. Hemminger and H.-J. Flammersheim, “Differential Scanning Calorimetry,” 2nd Edition, Springer, Heidelberg, 2010, pp. 71-91.[2] F. J. Stevenson, “Humus Chemistry: Genesis, Composition, Reactions,” 2nd Edition, Wiley, 1994, pp. 188-208.[3] J. H. Flynn and L. A. Wall, “A Quick, Direct Method for the Determination of Activation Energy from Thermogravimetric Data,” Polymer Letters Vol. 4, No. 5, 1966, pp. 323-328. http://dx.doi.org/10.1002/pol.1966.110040504[4] ASTM Test Method E1641, “Standard Test Method for Decomposition Kinetics by Thermogravimetry,” ASTM Book of Standards 14.02, American Society for Testing and Materials, 1994, pp. 1042-1046.[5] D. J. 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