Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants

Analytical methodologies based on GC and HPLC were developed for the separation and quantification of carnosic acid, ursolic acid, caffeic acid, p-coumaric acid, rosmarinic acid, apigenin, luteolin, quercetin, kaempferol, naringenin, and pinocembrin. These methods were used to characterize essential...

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Fecha de publicación:
2012
Institución:
Ministerio de Ciencia Tecnología e Innovación
Repositorio:
Repositorio Institucional de Minciencias
Idioma:
eng
OAI Identifier:
oai:repositorio.minciencias.gov.co:20.500.14143/34165
Acceso en línea:
http://repositorio.colciencias.gov.co/handle/11146/34165
Palabra clave:
Aceites vegetales
Étanol
Biología vegetal
Essential oil
Flavonoid
Lippia
Origanoides
Supercritical fluid extraction
Aceites esenciales
Bioquímica vegetal
Tecnología química
Química agrícola
Catalizadores
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http://purl.org/coar/access_right/c_f1cf
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network_name_str Repositorio Institucional de Minciencias
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spelling Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plantsAceites vegetalesÉtanolBiología vegetalEssential oilFlavonoidLippiaOriganoidesSupercritical fluid extractionAceites esencialesBioquímica vegetalTecnología químicaQuímica agrícolaCatalizadoresAnalytical methodologies based on GC and HPLC were developed for the separation and quantification of carnosic acid, ursolic acid, caffeic acid, p-coumaric acid, rosmarinic acid, apigenin, luteolin, quercetin, kaempferol, naringenin, and pinocembrin. These methods were used to characterize essential oils and extracts obtained by solvent (methanol) and by supercritical fluid (CO2) extraction from stems and leaves of Lippia (Verbenaceae family) aromatic plants (Lippia alba, Lippia origanoides, Lippia micromera, Lippia americana, Lippia graveolens, and Lippia citriodora). Supercritical CO2 extraction isolated solely pinocembrin and narigenin from three L. origanoides chemotypes. Solvent extracts possessed a more varied composition that additionally included apigenin, quercetin, and luteolin. Solvent extraction afforded higher overall flavonoid yields from all species in comparison with supercritical CO2 extraction. Pinocembrin was determined in L. origanoides extract at a concentration of 30 mg/g of plant material, which is more than ten times higher than the amount at which polyphenols are regularly found in aromatic plant extracts.Departamento Administrativo de Ciencia, Tecnología e Innovación [CO] Colciencias5507-543-31904Programa: Bioprospección y desarrollo de ingredientes naturales para las industrias cosmética, farmacéutica y de productos de aseo con base en la biodiversidad colombianano2019-04-01T00:03:03Z2019-04-01T00:03:03Z2012-10-05info:eu-repo/date/embargoEnd/2024-01-31Artículo científicoinfo:eu-repo/semantics/articlehttp://purl.org/coar/version/c_970fb48d4fbd8a85http://purl.org/coar/resource_type/c_2df8fbb1pdf11 páginasapplication/pdfhttp://repositorio.colciencias.gov.co/handle/11146/34165Contiene 22 referencias bibliográficas. Véase documento adjunto10.1002/jssc.201200877J. Sep. Sci. 2013, 36, 192–202engPrograma: Bioprospección y desarrollo de ingredientes naturales para las industrias cosmética, farmacéutica y de productos de aseo con base en la biodiversidad colombiana. La publicación completa está disponible en : <a href="http://repositorio.colciencias.gov.co/handle/11146/34163" target="blank">http://repositorio.colciencias.gov.co/handle/11146/34163</a>Colombiahttp://purl.org/coar/access_right/c_f1cfStashenko, Elena E.Martínez Morales, Jairo RenéCala, Mónica P.Durán, Diego CamiloCaballero, Deyaniraoai:repositorio.minciencias.gov.co:20.500.14143/341652023-11-29T17:39:05Z
dc.title.none.fl_str_mv Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
title Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
spellingShingle Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
Aceites vegetales
Étanol
Biología vegetal
Essential oil
Flavonoid
Lippia
Origanoides
Supercritical fluid extraction
Aceites esenciales
Bioquímica vegetal
Tecnología química
Química agrícola
Catalizadores
title_short Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
title_full Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
title_fullStr Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
title_full_unstemmed Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
title_sort Chromatographic and mass spectrometric characterization of essential oils and extracts from Lippia (Verbenaceae) aromatic plants
dc.subject.none.fl_str_mv Aceites vegetales
Étanol
Biología vegetal
Essential oil
Flavonoid
Lippia
Origanoides
Supercritical fluid extraction
Aceites esenciales
Bioquímica vegetal
Tecnología química
Química agrícola
Catalizadores
topic Aceites vegetales
Étanol
Biología vegetal
Essential oil
Flavonoid
Lippia
Origanoides
Supercritical fluid extraction
Aceites esenciales
Bioquímica vegetal
Tecnología química
Química agrícola
Catalizadores
description Analytical methodologies based on GC and HPLC were developed for the separation and quantification of carnosic acid, ursolic acid, caffeic acid, p-coumaric acid, rosmarinic acid, apigenin, luteolin, quercetin, kaempferol, naringenin, and pinocembrin. These methods were used to characterize essential oils and extracts obtained by solvent (methanol) and by supercritical fluid (CO2) extraction from stems and leaves of Lippia (Verbenaceae family) aromatic plants (Lippia alba, Lippia origanoides, Lippia micromera, Lippia americana, Lippia graveolens, and Lippia citriodora). Supercritical CO2 extraction isolated solely pinocembrin and narigenin from three L. origanoides chemotypes. Solvent extracts possessed a more varied composition that additionally included apigenin, quercetin, and luteolin. Solvent extraction afforded higher overall flavonoid yields from all species in comparison with supercritical CO2 extraction. Pinocembrin was determined in L. origanoides extract at a concentration of 30 mg/g of plant material, which is more than ten times higher than the amount at which polyphenols are regularly found in aromatic plant extracts.
publishDate 2012
dc.date.none.fl_str_mv 2012-10-05
2019-04-01T00:03:03Z
2019-04-01T00:03:03Z
info:eu-repo/date/embargoEnd/2024-01-31
dc.type.none.fl_str_mv Artículo científico
info:eu-repo/semantics/article
dc.type.coarversion.fl_str_mv http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.coar.fl_str_mv http://purl.org/coar/resource_type/c_2df8fbb1
dc.identifier.none.fl_str_mv http://repositorio.colciencias.gov.co/handle/11146/34165
Contiene 22 referencias bibliográficas. Véase documento adjunto
10.1002/jssc.201200877
url http://repositorio.colciencias.gov.co/handle/11146/34165
identifier_str_mv Contiene 22 referencias bibliográficas. Véase documento adjunto
10.1002/jssc.201200877
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Programa: Bioprospección y desarrollo de ingredientes naturales para las industrias cosmética, farmacéutica y de productos de aseo con base en la biodiversidad colombiana. La publicación completa está disponible en : <a href="http://repositorio.colciencias.gov.co/handle/11146/34163" target="blank">http://repositorio.colciencias.gov.co/handle/11146/34163</a>
dc.rights.coar.fl_str_mv http://purl.org/coar/access_right/c_f1cf
rights_invalid_str_mv http://purl.org/coar/access_right/c_f1cf
dc.format.none.fl_str_mv pdf
11 páginas
application/pdf
dc.coverage.none.fl_str_mv Colombia
dc.source.none.fl_str_mv J. Sep. Sci. 2013, 36, 192–202
institution Ministerio de Ciencia Tecnología e Innovación
repository.name.fl_str_mv
repository.mail.fl_str_mv
_version_ 1860676505379536896